In situ neutron powder diffraction and structure determination in controlled humidities

被引:16
|
作者
Ting, Valeska P. [1 ]
Henry, Paul F. [2 ]
Schmidtmann, Marc [3 ]
Wilson, Chick C. [3 ]
Weller, Mark T. [1 ]
机构
[1] Univ Southampton, Sch Chem, Southampton SO9 5NH, Hants, England
[2] Helmholtz Zentrum Berlin Mat & Energie, MI 1, Berlin, Germany
[3] Univ Glasgow, Dept Chem, WestCHEM, Glasgow G12 8QQ, Lanark, Scotland
基金
英国工程与自然科学研究理事会;
关键词
CRYSTAL-STRUCTURE; X-RAY; WATER;
D O I
10.1039/b918702b
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A controlled-humidity sample environment has been constructed, allowing bulk powder samples undergoing humidity-induced phase transitions and reactions to be studied via in situ neutron diffraction. Associated developments in data collection and analysis permit this to be achieved without the use of D2O.
引用
收藏
页码:7527 / 7529
页数:3
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