In situ neutron powder diffraction and structure determination in controlled humidities

被引:16
|
作者
Ting, Valeska P. [1 ]
Henry, Paul F. [2 ]
Schmidtmann, Marc [3 ]
Wilson, Chick C. [3 ]
Weller, Mark T. [1 ]
机构
[1] Univ Southampton, Sch Chem, Southampton SO9 5NH, Hants, England
[2] Helmholtz Zentrum Berlin Mat & Energie, MI 1, Berlin, Germany
[3] Univ Glasgow, Dept Chem, WestCHEM, Glasgow G12 8QQ, Lanark, Scotland
基金
英国工程与自然科学研究理事会;
关键词
CRYSTAL-STRUCTURE; X-RAY; WATER;
D O I
10.1039/b918702b
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A controlled-humidity sample environment has been constructed, allowing bulk powder samples undergoing humidity-induced phase transitions and reactions to be studied via in situ neutron diffraction. Associated developments in data collection and analysis permit this to be achieved without the use of D2O.
引用
收藏
页码:7527 / 7529
页数:3
相关论文
共 50 条
  • [1] High temperature in situ neutron powder diffraction of oxides
    Tamimi, Mazin A.
    McIntosh, Steven
    JOURNAL OF MATERIALS CHEMISTRY A, 2014, 2 (17) : 6015 - 6026
  • [2] In situ neutron powder diffraction studies
    Goonetilleke, Damian
    Sharma, Neeraj
    PHYSICAL SCIENCES REVIEWS, 2021, 6 (03)
  • [3] Structure determination from powder diffraction
    Chernyshev, VV
    RUSSIAN CHEMICAL BULLETIN, 2001, 50 (12) : 2273 - 2292
  • [4] Structure determination from powder diffraction
    V. V. Chernyshev
    Russian Chemical Bulletin, 2001, 50 : 2273 - 2292
  • [5] β-SrNH and β-SrND -: Synthesis and crystal structure determination by X-ray and neutron powder diffraction
    Schultz-Coulon, V
    Irran, E
    Putz, B
    Schnick, W
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1999, 625 (07): : 1086 - 1092
  • [6] Distribution of hydrogen in metal hydrides studied by in situ powder neutron diffraction
    Nakamura, Yumiko
    Nakamura, Jin
    Iwase, Kenji
    Akiba, Etsuo
    NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2009, 600 (01) : 297 - 300
  • [7] Characterization of the structure of YD3 by neutron powder diffraction
    Udovic, TJ
    Huang, Q
    Rush, JJ
    JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1996, 57 (04) : 423 - 435
  • [8] Neutron powder diffraction determination of the magnetic structure of Gd3Ag4Sn4
    Cadogan, J. M.
    Ryan, D. H.
    Napoletano, M.
    Riani, P.
    Cranswick, L. M. D.
    JOURNAL OF PHYSICS-CONDENSED MATTER, 2009, 21 (12)
  • [9] The kinetics of bulk hydration of the disaccharides α-lactose and trehalose by in situ neutron powder diffraction
    Ting, Valeska P.
    Schmidtmann, Marc
    Henry, Paul F.
    Dann, Sandie E.
    Crisp, Jenna L.
    Wilson, Chick C.
    Weller, Mark T.
    MEDCHEMCOMM, 2010, 1 (05) : 345 - 348
  • [10] Neutron diffraction structure determination of NaAlD4
    Hauback, BC
    Brinks, HW
    Jensen, CM
    Murphy, K
    Maeland, AJ
    JOURNAL OF ALLOYS AND COMPOUNDS, 2003, 358 (1-2) : 142 - 145