1,3-Dimethyl-5-(thiazol-2-yldiazenyl)pyrimidine-2,4,6(1H,3H,5H)-trione

被引:2
作者
Seferoglu, Zeynel
Hokelek, Tuncer [1 ]
Sahin, Ertan
Celik, Mehmet Emin
Ertan, Nermin
机构
[1] Hacettepe Univ, Dept Phys, TR-06800 Ankara, Turkey
[2] Gazi Univ, Dept Chem, TR-06500 Ankara, Turkey
[3] Ataturk Univ, Dept Chem, TR-22240 Erzurum, Turkey
关键词
D O I
10.1107/S1600536806049816
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the molecule of the title compound, C9H9N5O3S, the thiazole ring is oriented with respect to the barbituric acid ring at a dihedral angle of 10.53 (7)degrees. In the crystal structure, intermolecular N-H...N hydrogen bonds link the molecules into centrosymmetric dimers; these dimers are arranged in sheets parallel to the ac plane.
引用
收藏
页码:O5855 / O5857
页数:3
相关论文
共 21 条
[1]   TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].
ALLEN, FH ;
KENNARD, O ;
WATSON, DG ;
BRAMMER, L ;
ORPEN, AG ;
TAYLOR, R .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19
[2]   Structures, vibrational frequencies, and normal modes of substituted azo dyes: Infrared, Raman, and density functional calculations [J].
Biswas, N ;
Umapathy, S .
JOURNAL OF PHYSICAL CHEMISTRY A, 2000, 104 (12) :2734-2745
[3]   AN EMPIRICAL CORRECTION FOR ABSORPTION ANISOTROPY [J].
BLESSING, RH .
ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 :33-38
[4]   SIMPLE NEW METHOD FOR THE SYNTHESIS OF 5-DEAZA-10-OXAFLAVIN, A POTENTIAL ORGANIC OXIDANT [J].
CHEN, X ;
TANAKA, K ;
YONEDA, F .
CHEMICAL & PHARMACEUTICAL BULLETIN, 1990, 38 (02) :307-311
[5]   Antibacterial Co(II), Cu(II), Ni(II) and Zn(II) complexes of thiadiazole derived furanyl, thiophenyl and pyrrolyl Schiff bases [J].
Chohan, ZH ;
Pervez, H ;
Rauf, A ;
Scozzafava, A ;
Supuran, CT .
JOURNAL OF ENZYME INHIBITION AND MEDICINAL CHEMISTRY, 2002, 17 (02) :117-122
[6]   THE RELATION BETWEEN LIGAND STRUCTURES, COORDINATION STEREOCHEMISTRY, AND ELECTRONIC AND THERMODYNAMIC PROPERTIES [J].
COMBA, P .
COORDINATION CHEMISTRY REVIEWS, 1993, 123 (1-2) :1-48
[8]  
Farrugia L. J., 1999, J. Appl. Crystallogr, V32, P837, DOI DOI 10.1107/S0021889899006020
[9]  
Gulliya K.S.U.S., 1999, US Patent, Patent No. [U.S. Patent 5,869,494, 5869494, 5869494A]
[10]   2ND ORDER HYPERPOLARIZABILITIES OF BARBITURIC-ACID DERIVATIVES [J].
IKEDA, H ;
KAWABE, Y ;
SAKAI, T ;
KAWASAKI, K .
CHEMISTRY LETTERS, 1989, (10) :1803-1806