Crystal structure of (tris(2-pyridylmethyl)amine-κ4N,N′,N'',N'''')-chloranilato-κO,O′-zinc(II) - methanol (1/1), C25H22Cl2N4O5Zn

被引:1
作者
Zhao Yun [1 ]
Xu Lu [1 ]
Zhang Li-Fang [1 ]
机构
[1] China Univ Min & Technol, Sch Chem Engn & Technol, Xuzhou 221116, Jiangsu, Peoples R China
来源
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2017年 / 232卷 / 02期
关键词
MAGNETIC-PROPERTIES; COMPLEXES;
D O I
10.1515/ncrs-2016-0237
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C25H22Cl2N4O5Zn, monoclinic, P2(1)/c (no. 14), a = 16.302(3) angstrom, b = 11.324(2) angstrom, c = 14.636(3) angstrom, beta = 111.43(3)degrees, V = 2515.1(9) angstrom(3), Z = 4, R-gt(F) = 0.0511, wR(ref)(F-2) = 0.1109, T = 123(2) K.
引用
收藏
页码:275 / 277
页数:3
相关论文
共 11 条
[1]   Structural Diversity and Physical Properties of Paramagnetic Molecular Conductors Based on Bis(ethylenedithio)tetrathiafulvalene (BEDT-TTF) and the Tris(chloranilato)ferrate(III) Complex [J].
Atzori, Matteo ;
Pop, Flavia ;
Auban-Senzier, Pascale ;
Gomez-Garcia, Carlos J. ;
Canadell, Enric ;
Artizzu, Flavia ;
Serpe, Angela ;
Deplano, Paola ;
Avarvari, Narcis ;
Mercuri, Maria Laura .
INORGANIC CHEMISTRY, 2014, 53 (13) :7028-7039
[2]   Synthesis, crystal structure and valence tautomerism of a 4,4′-bipyridine-bridged one-dimensional chiral cobalt complex [J].
Cheng, Wei-Qin ;
Li, Guo-Ling ;
Zhang, Ran ;
Ni, Zhong-Hai ;
Wang, Wen-Feng ;
Sato, Osamu .
JOURNAL OF MOLECULAR STRUCTURE, 2015, 1087 :68-72
[3]   Syntheses and crystal structures of four cyanide-bridged trinuclear iron(III)-copper(II)-iron(III) complexes exhibiting abnormal antiferromagnetic coupling [J].
Ji, Yujie ;
Zhang, Lifang ;
Zhao, Yun ;
Ni, Zhonghai .
TRANSITION METAL CHEMISTRY, 2015, 40 (04) :437-444
[4]   Crystal structure of (tris(1-pyrazolylethyl)amine-κ4N,N′N",N′′′)-silver(I)] hexafluorophosphate, [Ag(C15H21N7](PF6) [J].
Ni, Zhong-Hai ;
Li, Guo-Ling ;
Nie, Jing .
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2011, 226 (04) :579-580
[5]   Syntheses, Structures and Magnetic Properties of Dinuclear Cobalt(II) Complexes [Co2(TPEA)2(DHBQ)](ClO4)2 and [Co2(TPEA)2(DHBQ)](PF6)2 [J].
Nie, Jing ;
Li, Guo-Ling ;
Miao, Bao-Xi ;
Ni, Zhong-Hai .
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2013, 43 (06) :331-334
[6]   Control of magnetic properties through external stimuli [J].
Sato, Osamu ;
Tao, Jun ;
Zhang, Yuan-Zhu .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2007, 46 (13) :2152-2187
[7]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[8]   SYNTHESIS AND CHARACTERIZATION OF STERICALLY HINDERED CUN4 COMPLEXES OF TRIPOD LIGANDS [J].
SORRELL, TN ;
JAMESON, DL .
INORGANIC CHEMISTRY, 1982, 21 (03) :1014-1019
[9]   Single-crystal structure validation with the program PLATON [J].
Spek, AL .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :7-13
[10]  
Zhang LF, 2016, CHINESE J INORG CHEM, V32, P731