(1R,2S,3R,5S)-5-(1H-Benzimidazol-2-yl)cyclohexane-1,2,3,5-tetraol monohydrate

被引：0

作者：

Cai, Ying ^{[1
]}

机构：

[1] Southeast Univ, Ordered Matter Sci Res Ctr, Nanjing 211189, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷

关键词：

D O I：

10.1107/S1600536809037957

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the crystal structure of the title compound, C13H16N2O4 center dot-H2O, intermolecular N-H center dot center dot center dot O, O-H center dot center dot center dot O and O-H center dot center dot center dot N hydrogen bonds form an extensive three-dimensional network, consolidating the crystal packing. The cyclohexane ring adopts a chair conformation.

引用

页码：O2547 / +

页数：9

共 8 条

[1]

[Anonymous], 2005, CRYSTALCLEAR

[2] GENERAL DEFINITION OF RING PUCKERING COORDINATES [J].

CREMER, D ;

POPLE, JA .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (06) :1354-1358

[3] Intermolecular interactions in two (ferrocenylmethyl)benzimidazoles incorporating the 4-MeOC6H4 and 3,4-(MeO)2C6H3 groups:: analysis of MeO-C-C distortions from ideal 120° geometry [J].

Gallagher, JF ;

Hanlon, K ;

Howarth, J .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2001, 57 (57) :1410-1414

[4]

HOWARTH J, 2001, TETRAHEDRON LETT, V42, P271

[5] [Zn(bim)2] • (H2O)1.67:: A metalorganic open-framework with sodalite topology [J].

Huang, XC ;

Zhang, JP ;

Chen, XM .

CHINESE SCIENCE BULLETIN, 2003, 48 (15) :1531-1534

[6] Synthesis, crystal and molecular structures of 1-n-butyl-2-(3′-chlorophenyl)-1H-benzimidazole-5-carbonitrile hemihydrate and 1-n-butyl-2-(3′,4′-dimethoxyphenyl)-1H-benzimidazole-5-carbonitrile [J].

Kazak, C. ;

Yilmaz, V. T. ;

Goker, H. ;

Kus, C. .

CRYSTAL RESEARCH AND TECHNOLOGY, 2006, 41 (05) :528-532

[7] Co-ordination chemistry of bis(ferrocenylcarbaldimine) Schiff bases [J].

Li, PY ;

Scowen, IJ ;

Davies, JE ;

Halcrow, MA .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1998, (22) :3791-3799

[8] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

← 1 →