Synthesis and Crystal Structure of Complex [La(p-OHC6H4CH2COO)3(phen)]2•2H2O

被引：0
作者：
Xian Chun-Ying [1 ]
Lin Miao [1 ]
Pan Wen-Li [1 ]
机构：
[1] Donghua Univ, Key Lab Sci & Technol Eco Text, Minist Educ, Shanghai 201620, Peoples R China
来源：
CHINESE JOURNAL OF INORGANIC CHEMISTRY | 2009年 / 25卷 / 07期
关键词：
complex; synthesis; crytal structure;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A complex of lanthanides formulated as [La(p-OHC6H4CH2COO)(3)(phen)](2) was prepared from the water/ethanol solution under normal temperturate with 8-hydroxyquinoline as the acidity conditionor, the complex was characterized by elemental analysis, IR, H-1 NMR spectroscopy and X-ray crystal structure analysis. The crystal belongs to monoclinic crystal system, space group P2(1)/n,. The 1,10-phenanthroline and 4-hydroxyphenylacetic ligands coordinated to the center ion through O or N atoms. The structural feature of the complex were discussed. CCDC: 25305.
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页码：1308 / 1311
页数：4
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