Novel composite films prepared by sol-gel technology for the corrosion protection of AZ91D magnesium alloy

被引:23
作者
Zhang, Shiyan [1 ]
Li, Qing [1 ]
Fan, Jiaman [1 ]
Kang, Wei [1 ]
Hu, Wei [2 ]
Yang, Xiaokui [3 ]
机构
[1] Southwest Univ, Sch Chem & Chem Engn, Chongqing 400715, Peoples R China
[2] Natl Engn Res Ctr Instrument Funct Mat, Chongqing 400700, Peoples R China
[3] Southwest Univ, Sch Mat Sci & Engn, Chongqing 400715, Peoples R China
关键词
Magnesium alloy; Sol-gel process; Composite films; FT-IR; Corrosion; ELECTROCHEMICAL IMPEDANCE SPECTROSCOPY; COATINGS; BEHAVIOR; RESISTANCE;
D O I
10.1016/j.porgcoat.2009.08.011
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
A novel composite films technology was developed to improve the anticorrosion performance of AZ91D magnesium alloy. The composite films were prepared via sol-gel method which is a simple application procedure within industry. The structure of xerogels and films, morphology of films were analyzed using thermo-gravimetric (TG) and differential thermal analysis (DTA), Fourier transformed infrared spectroscopy (FT-IR), X-ray diffraction (XRD) and scan electron microscopy (SEM). The anticorrosion performance of the sol-gel coated and uncoated samples in 3.5 wt.% NaCl neutral solution had been evaluated by electrochemical tests. The results demonstrated that the composite films "Ce inner film/Mg outer film" exhibited better corrosion resistance. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:328 / 335
页数:8
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