Atomic-absorption determination of impurities in metallic mercury

被引:0
作者
Telegin, GF [1 ]
Shilkina, NN [1 ]
Grazhulene, SS [1 ]
机构
[1] Russian Acad Sci, Inst Engn Problems Microelect & Ultra Pure Met, Chernogolovka 142432, Moscow Dist, Russia
来源
INDUSTRIAL LABORATORY | 1999年 / 65卷 / 09期
关键词
D O I
暂无
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A method for atomic-absorption determination of 17 types of microimpurities in high-purity mercury at a detection limit of 10(-6) - 10(-7) wt.% is described. The method is based on preliminary concentration df impurities in solution, reduction of mercury ions to the elemental state with formic acid, and separation of mercury from the concentrate. The method is checked for correctness by a recovery test ("added - found"). The relative standard deviation is 0.03 - 0.07.
引用
收藏
页码:573 / 575
页数:3
相关论文
共 11 条
[1]  
CHAPYSHEVA TA, 1979, NEW METHODS INSTRUME, P35
[2]  
FURMAN NH, 1948, WASH ACAD SCI, V38, P159
[3]  
GILBERT EN, 1980, ZH ANAL KHIM, V35, P2300
[4]  
GORBACHEVA AM, 1959, T LEN POL I, P77
[5]  
JACKWERTH E, 1964, Z ANAL CHEM, V202, P81
[6]  
KARABASH AG, 1967, THESIS GEOFKHI MOSCO
[7]  
KUZMIN NM, Patent No. 160900
[8]  
LIPEEVA SI, 1996, ZAVODSK LAB, V62, P12
[9]  
MEYER J, 1966, Z ANAL CHEM FRESENIU, V219, P147
[10]  
NEIMAN EY, 1969, ZAVODSK LAB, V35, P277