3D Electron Diffraction: The Nanocrystallography Revolution

被引：439

作者：

Gemmi, Mauro ^{[1
]}

Mugnaioli, Enrico ^{[1
]}

Gorelik, Tatiana E. ^{[2
]}

Kolb, Ute ^{[3
,4
]}

Palatinus, Lukas ^{[5
]}

Boullay, Philippe ^{[6
]}

Hovmoller, Sven ^{[7
]}

Abrahams, Jan Pieter ^{[8
,9
,10
]}

机构：

[1] Ist Italiano Tecnol, Ctr Nanotechnol Innovat NEST, Piazza S Silvestro 12, I-56127 Pisa, Italy

[2] Univ Ulm, Cent Facil Electron Microscopy, Electron Microscopy Grp Mat Sci EMMS, Albert Einstein Allee 11, D-89081 Ulm, Germany

[3] Johannes Gutenberg Univ Mainz, Inst Anorgan Chem & Analyt Chem, Duesbergweg 10-14, D-55128 Mainz, Germany

[4] Tech Univ Darmstadt, Inst Angew Geowissensch, Schnittspahnstr 9, D-64287 Darmstadt, Germany

[5] CAS, Inst Phys, Dept Struct Anal, Prague 18221 8, Czech Republic

[6] Normandie Univ, ENSICAEN, CRISMAT, UNICAEN,CNRS UMR 6508, 6 Bd Marechal Juin, F-14050 Caen, France

[7] Stockholm Univ, Dept Mat & Environm Chem, Inorgan & Struct Chem, S-10691 Stockholm, Sweden

[8] Basel Univ, Biozentrum, Ctr Cellular Imaging & NanoAnalyt C CINA, Mattenstr 26, CH-4058 Basel, Switzerland

[9] Paul Scherrer Inst, Dept Biol & Chem, CH-5232 Villigen, Switzerland

[10] Leiden Univ, Leiden Inst Biol, Sylviusweg 72, NL-2333 BE Leiden, Netherlands

来源：

ACS CENTRAL SCIENCE | 2019年 / 5卷 / 08期

关键词：

INITIO STRUCTURE DETERMINATION; INCOMMENSURATELY MODULATED STRUCTURE; CRYSTAL-STRUCTURE DETERMINATION; AB-INITIO; ATOMIC-RESOLUTION; DATA-COLLECTION; CRYO-EM; STRUCTURAL-CHARACTERIZATION; PROTEIN CRYSTALS; TOMOGRAPHY;

D O I：

10.1021/acscentsci.9b00394

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Crystallography of nanocrystalline materials has witnessed a true revolution in the past 10 years, thanks to the introduction of protocols for 3D acquisition and analysis of electron diffraction data. This method provides single-crystal data of structure solution and refinement quality, allowing the atomic structure determination of those materials that remained hitherto unknown because of their limited crystallinity. Several experimental protocols exist, which share the common idea of sampling a sequence of diffraction patterns while the crystal is tilted around a noncrystallographic axis, namely, the goniometer axis of the transmission electron microscope sample stage. This Outlook reviews most important 3D electron diffraction applications for different kinds of samples and problematics, related with both materials and life sciences. Structure refinement including dynamical scattering is also briefly discussed.

引用

页码：1315 / 1329

页数：15

共 168 条

[1] Structure of the Yeast Mitochondrial Large Ribosomal Subunit [J].

Amunts, Alexey ;

Brown, Alan ;

Bai, Xiao-chen ;

Llacer, Jose L. ;

Hussain, Tanweer ;

Emsley, Paul ;

Long, Fei ;

Murshudov, Garib ;

Scheres, Sjors H. W. ;

Ramakrishnan, V. .

SCIENCE, 2014, 343 (6178) :1485-1489

[2] The Crystal Structure of Orthocetamol Solved by 3D Electron Diffraction [J].

Andrusenko, Iryna ;

Hamilton, Victoria ;

Mugnaioli, Enrico ;

Lanza, Arianna ;

Hall, Charlie ;

Potticary, Jason ;

Hall, Simon R. ;

Gemmi, Mauro .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2019, 58 (32) :10919-10922

[3] Structure analysis of titanate nanorods by automated electron diffraction tomography [J].

Andrusenko, Iryna ;

Mugnaioli, Enrico ;

Gorelik, Tatiana E. ;

Koll, Dominik ;

Panthoefer, Martin ;

Tremel, Wolfgang ;

Kolb, Ute .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2011, 67 :218-225

[4] Formation of Hydrous, Pyroxene-Related Phases from LiAlSiO4 Glass in High-Pressure Hydrothermal Environments [J].

Angstrom, Jonas ;

Jenei, Istvan Zoltan ;

Spektor, Kristina ;

Haussermann, Ulrich .

ACS EARTH AND SPACE CHEMISTRY, 2019, 3 (01) :8-16

[5]

[Anonymous], 2007, Aperiodic Crystals: From Modulated Phases to Quasicrystals

[6]

Arndt U.W., 1977, The Rotation Method in Crystallography: Data Collection from Macromolecular Crystals

[7] Eu Incorporation into Sol-Gel Silica for Photonic Applications: Spectroscopic and TEM Evidences of α-Quartz and Eu Pyrosilicate Nanocrystal Growth [J].

Baraldi, Andrea ;

Buffagni, Elisa ;

Capelletti, Rosanna ;

Mazzera, Margherita ;

Fasoli, Mauro ;

Lauria, Alessandro ;

Moretti, Federico ;

Vedda, Anna ;

Gemmi, Mauro .

JOURNAL OF PHYSICAL CHEMISTRY C, 2013, 117 (50) :26831-26848

[8] ECS-3: A Crystalline Hybrid Organic-Inorganic Aluminosilicate with Open Porosity [J].

Bellussi, Giuseppe ;

Montanari, Erica ;

Di Paola, Eleonora ;

Millini, Roberto ;

Carati, Angela ;

Rizzo, Caterina ;

Parker, Wallace O'Neil, Jr. ;

Gemmi, Mauro ;

Mugnaioli, Enrico ;

Kolb, Ute ;

Zanardi, Stefano .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2012, 51 (03) :666-669

[9] New developments in the Inorganic Crystal Structure Database (ICSD): accessibility in support of materials research and design [J].

Belsky, A ;

Hellenbrandt, M ;

Karen, VL ;

Luksch, P .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 2002, 58 :364-369

[10] High-Pressure Synthesis of Novel Boron Oxynitride B6N4O3 with Sphalerite Type Structure [J].

Bhat, Shrikant ;

Wiehl, Leonore ;

Molina-Luna, Leopoldo ;

Mugnaioli, Enrico ;

Lauterbach, Stefan ;

Sicolo, Sabrina ;

Kroll, Peter ;

Duerrschnabel, Michael ;

Nishiyama, Norimasa ;

Kolb, Ute ;

Albe, Karsten ;

Kleebe, Hans-Joachim ;

Riedel, Ralf .

CHEMISTRY OF MATERIALS, 2015, 27 (17) :5907-5914

← 1 2 3 4 5 6 7 8 9 10 →