Analysis of Parent/Nitrated Polycyclic Aromatic Hydrocarbons in Particulate Matter 2.5 Based on Femtosecond Ionization Mass Spectrometry

被引：11
|
作者：
Itouyama, Noboru [1 ]
Matsui, Taiki [1 ]
Yamamoto, Shigekazu [2 ]
Imasaka, Tomoko [3 ]
Imasaka, Totaro [1 ,4 ]
机构：
[1] Kyushu Univ, Grad Sch Engn, Dept Appl Chem, Nishi Ku, Fukuoka 8190395, Japan
[2] Fukuoka Inst Hlth & Environm Sci, Dazaifu, Fukuoka 8180135, Japan
[3] Kyushu Univ, Grad Sch Design, Chem Lab, Minami Ku, Fukuoka 8158540, Japan
[4] Kyushu Univ, Div Optoelect & Photon, Ctr Future Chem, Nishi Ku, Fukuoka 8190395, Japan
来源：
JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY | 2016年 / 27卷 / 02期
基金：
日本学术振兴会;
关键词：
Gas chromatography; Multiphoton ionization; Time-of-flight mass spectrometry; Particulate matter 2.5; Polycyclic aromatic hydrocarbons; Nitrated polycyclic aromatic hydrocarbons; 2-DIMENSIONAL GAS-CHROMATOGRAPHY; ON-SITE ANALYSIS; MULTIPHOTON IONIZATION; STANDARD; DIOXIN; LASER; PAHS; 1-NITROPYRENE; SOOT; AIR;
D O I：
10.1007/s13361-015-1276-x
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Particulate matter 2.5 (PM2.5), collected from ambient air in Fukuoka City, was analyzed by gas chromatography combined with multiphoton ionization mass spectrometry using an ultraviolet femtosecond laser (267 nm) as the ionization source. Numerous parent polycyclic aromatic hydrocarbons (PPAHs) were observed in a sample extracted from PM2.5, and their concentrations were determined to be in the range from 30 to 190 pg/m(3) for heavy PPAHs. Standard samples of nitrated polycyclic aromatic hydrocarbons (NPAHs) were examined, and the limits of detection were determined to be in the picogram range. The concentration of NPAH adsorbed on PM2.5 in the air was less than 900-1300 pg/m(3).
引用
收藏
页码：293 / 300
页数：8
相关论文
共 50 条
  • [1] Multiphoton ionization mass spectrometry of nitrated polycyclic aromatic hydrocarbons
    Tang, Yuanyuan
    Imasaka, Tomoko
    Yamamoto, Shigekazu
    Imasaka, Totaro
    TALANTA, 2015, 140 : 109 - 114
  • [2] Trace analysis of nitrated polycyclic aromatic hydrocarbons based on two-color femtosecond laser ionization mass spectrometry
    Wen, Lu
    Yoshinaga, Katsunori
    Imasaka, Totaro
    Imasaka, Tomoko
    TALANTA, 2023, 265
  • [3] Determination of nitrated polycyclic aromatic hydrocarbons in particulate matter 2.5 by laser ionization mass spectrometry using an on-line chemical-reduction system
    Tang, Yuanyuan
    Yamamoto, Shigekazu
    Imasaka, Totaro
    ANALYST, 2019, 144 (09) : 2909 - 2913
  • [4] Use of chemical conversion for determination of nitrated aromatic hydrocarbons using femtosecond ionization mass spectrometry
    Fujii, Takuya
    Imasaka, Tomoko
    Imasaka, Totaro
    ANALYTICA CHIMICA ACTA, 2017, 996 : 48 - 53
  • [5] Pyrolysis-Gas Chromatography/Multiphoton Ionization/ Time-of-Flight Mass Spectrometry for the Rapid and Selective Analysis of Polycyclic Aromatic Hydrocarbons in Aerosol Particulate Matter
    Shunsuke Sakurai
    Tomohiro Uchimura
    Analytical Sciences, 2014, 30 : 891 - 895
  • [6] Pyrolysis-Gas Chromatography/Multiphoton Ionization/Time-of-Flight Mass Spectrometry for the Rapid and Selective Analysis of Polycyclic Aromatic Hydrocarbons in Aerosol Particulate Matter
    Sakurai, Shunsuke
    Uchimura, Tomohiro
    ANALYTICAL SCIENCES, 2014, 30 (09) : 891 - 895
  • [7] Determination of polycyclic aromatic hydrocarbons and their nitro-, amino-derivatives absorbed on particulate matter 2.5 by multiphoton ionization mass spectrometry using far-, deep-, and near-ultraviolet femtosecond lasers
    Tang, Yuanyuan
    Imasaka, Tomoko
    Yamamoto, Shigekazu
    Imasaka, Totaro
    CHEMOSPHERE, 2016, 152 : 252 - 258
  • [8] Simultaneous GC/MS analysis of polycyclic aromatic hydrocarbons and their nitrated derivatives in atmospheric particulate matter from workplaces
    Chaspoul, F
    Barban, G
    Gallice, P
    POLYCYCLIC AROMATIC COMPOUNDS, 2005, 25 (02) : 157 - 167
  • [9] Simultaneous determination of polycyclic aromatic dydrocarbons and their nitrated derivatives in airborne particulate matter using gas chromatography-tandem mass spectrometry
    Nicol, S
    Dugay, J
    Hennion, MC
    JOURNAL OF SEPARATION SCIENCE, 2001, 24 (06): : 451 - 458
  • [10] Characterization and Identification of Polycyclic Aromatic Hydrocarbons in Diesel Particulate Matter
    Kanaujia, Pankaj K.
    Singh, Devendra
    Tripathi, Deependra
    Konathala, L. N. Siva Kumar
    Saran, Sandeep
    Chauhan, R. K.
    Sharma, Yogendra K.
    Garg, Madhukar O.
    ANALYTICAL LETTERS, 2015, 48 (14) : 2303 - 2318
12345