1-Bromo-2,7-di-tert-butylpyrene

被引:0
作者
Xia, Guang-Ming [1 ]
Liu, Zhi-Qiang [2 ]
Lu, Ping [1 ]
Sun, Guo-Xin [1 ]
Chen, Hong-Yu [3 ]
机构
[1] Univ Jinan, Sch Chem & Chem Engn, Jinan 250022, Peoples R China
[2] Shandong Univ, State Key Lab Crystal Mat, Jinan 250100, Shandong, Peoples R China
[3] TaiShan Med Univ, Sch Chem & Chem Engn, Tai An 271016, Shandong, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词
CRYSTAL-STRUCTURE;
D O I
10.1107/S1600536809054257
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title molecule, C(24)H(25)Br, one of two tert-butyl groups is rotationally disordered between two orientations in a 0.59 (3):0.41 (3) ratio. The crystal packing exhibits no pi-pi interactions; however, relatively short intermolecular Br center dot center dot center dot Br contacts of 3.654 (1) angstrom are observed.
引用
收藏
页码:O216 / U2963
页数:10
相关论文
共 50 条
  • [21] Synthesis and Crystal Structure of Chiral (S,RFc)-N-1-(2-diphenylphosphino)ferrocenylethyl-2-hydroxyl-3,5-di-tert-butylbenzalimine
    Zhang, Yu-Mei
    Liu, Peng
    Zhang, Hong-Li
    Zhang, Li
    Zhou, Zhi-Ming
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2008, 38 (02) : 147 - 150
  • [22] Synthesis and crystal structure of 1,3-di-tert-butyl-2-chloro-4,4-diphenyl-1,3,2λ3,4-diazaphosphasiletudine
    Mo, Dennis
    Frank, Walter
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2019, 75 : 405 - +
  • [23] Synthesis, Structures, and Magnetic Behavior of Two Binuclear Fe(III) Complexes of N-(1-ethanol)-N,N-bis(3,5-di-tert-butyl-2-hydroxybenxyl)amine and N-(3-amino-1-propanol)-N,N-bis(3,5-di-tert-butyl-2-hydroxybenxyl)amine
    Yu, Gang
    Chen, Jin-Ye
    Cai, Zhan-Mao
    Zhan, Shu-Zhong
    SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2014, 44 (01) : 48 - 54
  • [24] Crystal structure of bis(eta(5)-cyclopentadienyl)(1,4-di-tert-butylbuta-1-en-3-yn-1yl)zirconium(IV) mu(2)-hydroxido-bis[tris(pentafluorophenyl)borate]
    Burlakov, Vladimir V.
    Spannenberg, Anke
    Arndt, Perdita
    Rosenthal, Uwe
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : M71 - +
  • [25] Synthesis and Crystal Structure of 4,6Di-tert-butyl-2-hydroxy-3-(N-1-phenylethyliminomethyl) phenyl bis(triphenylphosphine)palladium bromide
    XU JiaXi\ ZHANG ZeYing\= (College of Chemistry and Molecular Engineering
    结构化学, 1999, (04) : 54 - 59
  • [26] 1,3-Di-tert-butyl-6H-benzo[b]naphtho[1,2-d]pyran-6-thione, a severely helically distorted thionolactone-bridged biaryl
    Bringmann, G
    Wuzik, A
    Schupp, O
    Peters, K
    Peters, EM
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1997, 52 (03): : 355 - 358
  • [27] Synthesis, characterization, crystal structure and catalytic property of [Cu(SalAHE)2] (SalAHE = salicylaldehydeimine-1-hydroxyethane) complex for the oxidation of 3,5-di-tert-butylcatechol
    Midoes, Ana C. D.
    Aranha, Pedro E.
    dos Santos, Mirian P.
    Tozzo, Erica
    Romera, Sandra
    Santos, Regina H. de A.
    Dockal, Edward R.
    POLYHEDRON, 2008, 27 (01) : 59 - 64
  • [28] PHOTOCHROMIC AND THERMOCHROMIC MANNICH-BASES .1. MANNICH-BASES FROM 3,5-DI-TERT-BUTYL-4-HYDROXYBENZALDEHYDE AND 2-NAPHTHOLS
    KOMISSAROV, VN
    UKHIN, LY
    KHARLANOV, VA
    LOKSHIN, VA
    BULGAREVICH, EY
    MINKIN, VI
    FILIPENKO, OS
    NOVOZHILOVA, MA
    ALDOSHIN, SM
    ATOVMYAN, LO
    BULLETIN OF THE RUSSIAN ACADEMY OF SCIENCES-DIVISION OF CHEMICAL SCIENCE, 1992, 41 (10): : 1875 - 1883
  • [29] Crystal structure and Hirshfeld surface analysis of 5-(3,5-di-tert-butyl-4-hydroxyphenyl)-3-phenyl-4,5-dihydro-1H-pyrazole-1-carboxamide
    Asgarova, Ayten R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2019, 75 : 1467 - +
  • [30] 1,4-Addition of lithium organyls to para-quinols structure determination of 2,6-di-tert-butyl-4-hydroxy-4,5-diphenylcyclohex-2-en-1-one
    Henes, G
    Rieker, A
    Neumayer, M
    Hiller, W
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1996, 51 (03): : 381 - 387