Synthesis and crystal structure of a dinuclear titanium(IV) complex containing an allopyranosidato ligand

被引：5
|
作者：
Kuentzer, Daniela [1 ]
Tschersich, Sebastian [1 ]
Heck, Juergen [1 ]
机构：
[1] Univ Hamburg, Dept Chem, D-20146 Hamburg, Germany
来源：
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE | 2007年 / 633卷 / 01期
关键词：
titanium; dinuclear complexes; carbohydrate complexes;
D O I：
10.1002/zaac.200600235
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The reaction of methyl-4,6-O-benzylidene-alpha-D-allopyranoside (alpha-MeBAH(2)) with trichlorocyclopentadienyltitanium [CpTiCl3] and triethylamine in dichloromethane led to the dinuclear complex [(CpTiCl2)(2)-mu-(alpha-MeAG)] (1). 1 was characterized by elemental analysis, H-1 NMR spectroscopy as well as single crystal X-ray diffraction.
引用
收藏
页码：43 / 45
页数：3
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