High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment

被引：352

作者：

Vinogradov, E ^{[1
]}

Madhu, PK ^{[1
]}

Vega, S ^{[1
]}

机构：

[1] Weizmann Inst Sci, Dept Chem Phys, IL-76100 Rehovot, Israel

来源：

CHEMICAL PHYSICS LETTERS | 1999年 / 314卷 / 5-6期

基金：

以色列科学基金会;

关键词：

D O I：

10.1016/S0009-2614(99)01174-4

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

In this Letter, we present a pulse scheme for coherent averaging of spin-spin interactions called phase-modulated Lee-Goldburg (PMLG) which is aimed at achieving high-resolution proton NMR spectra in the solid state. Our objective is mainly to discuss the design and execution of this experiment and to show some preliminary experimental results as evidence of the far-reaching potentials of this technique. (C) 1999 Elsevier Science B.V. All rights reserved.

引用

页码：443 / 450

页数：8

共 29 条

[1] Broadband polarization transfer under magic-angle spinning: Application to total through-space-correlation NMR spectroscopy [J].

Baldus, M ;

Meier, BH .

JOURNAL OF MAGNETIC RESONANCE, 1997, 128 (02) :172-193

[2] FREQUENCY-SWITCHED PULSE SEQUENCES - HOMONUCLEAR DECOUPLING AND DILUTE SPIN NMR IN SOLIDS [J].

BIELECKI, A ;

KOLBERT, AC ;

LEVITT, MH .

CHEMICAL PHYSICS LETTERS, 1989, 155 (4-5) :341-346

[3]

Bielecki A., 1990, ADV MAGN RESON, V14, P111, DOI [10.1016/b978-0-12-025514-6.50011-3, DOI 10.1016/B978-0-12-025514-6.50011-3]

[4] COMBINED ROTATION AND MULTIPLE PULSE SPECTROSCOPY AS AN ANALYTICAL PROTON NUCLEAR MAGNETIC-RESONANCE TECHNIQUE FOR SOLIDS [J].

BRONNIMANN, CE ;

HAWKINS, BL ;

ZHANG, M ;

MACIEL, GE .

ANALYTICAL CHEMISTRY, 1988, 60 (17) :1743-1750

[5] ANALYSIS OF MULTIPLE PULSE NMR IN SOLIDS .3. [J].

BURUM, DP ;

RHIM, WK .

JOURNAL OF CHEMICAL PHYSICS, 1979, 71 (02) :944-956

[6] ISOTROPIC SPECTRA OF HALF-INTEGER QUADRUPOLAR SPINS FROM BIDIMENSIONAL MAGIC-ANGLE-SPINNING NMR [J].

FRYDMAN, L ;

HARWOOD, JS .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1995, 117 (19) :5367-5368

[7] 13C NMR of liquid crystals with different proton homonuclear dipolar decoupling methods [J].

Fung, BM ;

Ermolaev, K ;

Yu, YL .

JOURNAL OF MAGNETIC RESONANCE, 1999, 138 (01) :28-35

[8] UTILITY OF PULSE NUCLEAR MAGNETIC-RESONANCE IN STUDYING PROTONS IN COALS [J].

GERSTEIN, BC ;

CHOW, C ;

PEMBLETON, RG ;

WILSON, RC .

JOURNAL OF PHYSICAL CHEMISTRY, 1977, 81 (06) :565-570

[9]

Haeberlen U, 1976, ADV MAGN RESON

[10] Multiple-pulse line narrowing under fast magic-angle spinning [J].

Hafner, S ;

Spiess, HW .

JOURNAL OF MAGNETIC RESONANCE SERIES A, 1996, 121 (02) :160-166

← 1 2 3 →