Ultrafine-Grained Zn-Mg-Sr Alloy Synthesized by Mechanical Alloying and Spark Plasma Sintering

被引:5
作者
Necas, David [1 ]
Kubasek, Jiri [1 ]
Pinc, Jan [2 ]
Marek, Ivo [1 ]
Donik, Crtomir [3 ]
Paulin, Irena [3 ]
Vojtech, Dalibor [1 ]
机构
[1] Univ Chem & Technol, Fac Chem Technol, Dept Met & Corros Engn, Prague Tech 5, Prague 16628, Czech Republic
[2] Czech Acad Sci, Inst Phys, Dept Funct Mat, Slovance 1999-2, Prague 18221, Czech Republic
[3] Univ Ljubljana, Inst Met & Technol, Dept Phys & Chem Mat, Lepi Pot 11, SI-1000 Ljubljana, Slovenia
关键词
metals and alloys; biomaterials; mechanical alloying; sintering; nanostructure; compression test; BIODEGRADABLE ZINC-ALLOYS; MICROSTRUCTURE; MAGNESIUM; BEHAVIOR; STRATEGY; DESIGN;
D O I
10.3390/ma15238379
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Zinc materials are considered promising candidates for bioabsorbable medical devices used for the fixation of broken bones or stents. Materials for these applications must meet high mechanical property requirements. One of the ways to fulfil these demands is related to microstructure refinement, particularly the decrease in grain size. In the present work, we combine two powder metallurgy techniques (mechanical alloying-MA, and spark plasma sintering-SPS) to prepare Zn-1Mg-0.5Sr nanograin material. The microstructure of compacted material consisted of Zn grains and particles of Mg2Zn11 intermetallic phases from 100 to 500 nm in size, which resulted in high values of hardness and a compressive strength equal to 86 HV1 and 327 MPa, respectively. In this relation, the combination of the suggested techniques provides an innovative way to form extremely fine microstructures without significant coarsening during powder compaction at increased temperatures.
引用
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页数:11
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