Multi-scale characterisation of hybrid organic-inorganic materials using new solid-state NMR methods

Recent developments of high-resolution NMR techniques for proton in the solid state open the way to obtaining a more accurate description of the structure of proton containing materials at different length scales (from 0.1 up to 200 nm). This can be achieved through the combined use of Lee-Golburg homonuclear proton decoupling and proton spin-diffusion. In that scope we describe a multi-scale characterisation of a layered and phase-separated zinc phosphonate material.