A comparison of field assisted hot pressing and hot isostatic pressing for gas atomized Ti-22Al-26Nb(at.%) and Ti-22Al-26Nb-5B(at.%) powders

Ti-22Al-26Nb(at.%) and Ti-22Al-26Nb-5B(at.%) compacts were processed from gas atomized prealloyed powders by field assisted hot pressing (FAHP) for between 600 and 1200 s at temperatures between 725 and 1070 degrees C and the resulting microstructures were compared. The average powder diameters ranged between 50 and 100 mu m, where both the B-containing powders and resulting FAHP compacts contained elongated B-rich needles. The microstructure in the FAHP compacts depended on the processing temperature. For processing temperatures less than or equal to 960 degrees C, porosity was evident on the FAHP compact, where greater porosity was observed with decreasing temperature. Processing temperatures greater than or equal to 980 degrees C resulted in minimal porosity and three-phase microstructures containing a mixture of the orthorhombic, alpha(2), and body-centered-cubic (BCC) phases, where longer processing times led to microstructural coarsening. The microstructures of the FAHP compacts were compared to those from compacts consolidated at 1027 degrees C for 4 h using hot isostatic pressing (HIP). For both HIP and FAHP processing, the B-containing compacts exhibited finer prior-BCC grain sizes. Compositional analysis of the B-rich phase within the Ti-22Al-26Nb HIP compact suggested that it could be the B27 orthorhombic structure with a B2TiNb stoichiometry. Overall, FAHP was shown to be a viable powder metallurgy processing technique for intermetallic Ti2AlNb based intermetallic alloys. (C) 2020 Elsevier B.V. All rights reserved.