Rapid screening for anthocyanins and anthocyanin dimers in crude grape extracts by high performance liquid chromatography coupled with diode array detection and tandem mass spectrometry

被引：40
|
作者：
Pati, Sandra [1 ]
Liberatore, Maria Teresa [2 ]
Gambacorta, Giuseppe [1 ]
Antonacci, Donato [3 ]
La Notte, Ennio [1 ]
机构：
[1] Univ Foggia, Dept Food Sci, Foggia, Italy
[2] Univ Foggia, Prod Sci Engn & Econ Agr Syst Dept, Fac Agr, I-71100 Foggia, Italy
[3] CRA UTV, Unita Ric Uva Tavola & Vitivinicoltura Ambiente M, I-70010 Turi, BA, Italy
来源：
JOURNAL OF CHROMATOGRAPHY A | 2009年 / 1216卷 / 18期
关键词：
Anthocyanin; Dimers; Tandem mass spectrometry; Rapid resolution; High performance liquid chromatography; Grape; RED WINE; HPLC; IDENTIFICATION; ELECTROSPRAY; COLORANTS; STABILITY; CYANIDIN; JUICES; COLUMN; FOOD;
D O I：
10.1016/j.chroma.2009.02.068
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A rapid and efficient method using high performance liquid chromatography coupled with diode array detection and tandem mass spectrometry (HPLC-DAD-MS/MS) for fast screening large numbers of anthocyanins and anthocyanin dimers in different grape skin extracts, without further sample cleanup procedures, was developed. A good separation of most detected anthocyanins was achieved in a run time of 15 min. identification of anthocyanin pigments required a combination of several information: UV-vis spectra, MS and MS/MS spectra, and elution pattern. Many compounds have been here detected for the first time and their structures tentatively elucidated. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码：3864 / 3868
页数：5
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