Synthesis of (η6-arene)tricarbonylchromium derivatives of 1,4-dihydro-3,1-benzoxazines

被引：8

作者：

Sazonova, E., V ^{[1
]}

Artemov, A. N. ^{[1
]}

Faerman, V., I ^{[1
]}

Aksenova, N. A. ^{[1
]}

Timofeeva, A. A. ^{[1
]}

Zaytseva, Yu A. ^{[1
]}

Somov, N., V ^{[1
]}

Grishina, N. Yu ^{[1
]}

机构：

[1] Lobachevsky State Univ Nizhny Novgorod, 5 Korp,23 Prosp Gagarina, Nizhnii Novgorod 603950, Russia

来源：

RUSSIAN CHEMICAL BULLETIN | 2021年 / 70卷 / 01期

关键词：

(η (6)-arene)tricarbonylchromium; 1; 4-dihydro-3; 1-benzoxazines; heterocyclic compounds; triammine(tricarbonyl)chromium; 1,3-DIPOLAR CYCLOADDITION REACTION; PI-COMPLEXES; TRICARBONYL; 1,3-OXAZOLIDINES; ISOXAZOLIDINES; 1,3-OXAZINANES; CONDENSATION; ALDEHYDES; CHEMISTRY; DENSITY;

D O I：

10.1007/s11172-021-3073-y

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A series of (eta(6)-arene)tricarbonylchromium derivatives of 1,4-dihydro-3,1-benzoxazines was synthesized and characterized. The compounds were obtained by two alternative methods, namely, by the reaction of triammine(tricarbonyl)chromium with 1,4-dihydro-3,1-benzoxazines (method A) and by the condensation of (eta(6)-2-aminobenzyl alcohol)tricarbonylchromium with various aldehydes and ketones (method B). The composition and structure of obtained compounds were established by different physicochemical methods of analysis, such as HPLC, UV, IR, H-1 NMR spectroscopy, mass spectrometry, and X-ray diffraction.

引用

页码：171 / 178

页数：8

共 34 条

[1] Reaction of phenyl-containing N-substituted 1,3-oxazolidines and 1,3-oxazinanes with triammine(tricarbonyl)chromium [J].

Artemov, A. N. ;

Sazonova, E. V. ;

Aksenova, N. A. ;

Fukin, G. K. ;

Cherkasov, A. V. ;

Faerman, V. I. ;

Grishina, N. Yu. .

RUSSIAN CHEMICAL BULLETIN, 2019, 68 (08) :1548-1554

[2] The synthesis of new 1,3-oxazolidines and 1,3-oxazinanes containing (η6-arene)tricarbonylchromium group based on condensation between aldehydes and amino alcohols [J].

Artemov, A. N. ;

Sazonova, E. V. ;

Krylova, N. A. ;

Zvereva, E. A. ;

Pechen, N. A. ;

Fukin, G. K. ;

Cherkasov, A. V. ;

Faerman, V. I. ;

Grishina, N. Yu. .

RUSSIAN CHEMICAL BULLETIN, 2018, 67 (05) :884-892

[3] 1,3-Dipolar cycloaddition reaction of nitrone η6-(arene)chromium tricarbonyl complexes with styrene and η6-(styrene)chromium tricarbonyl [J].

Artemov, A. N. ;

Sazonova, E. V. ;

Zarovkina, N. Yu .

RUSSIAN CHEMICAL BULLETIN, 2013, 62 (06) :1382-1387

[4] Synthesis of new η6-(arene) chromium tricarbonyl complexes of isoxazolidines by 1,3-dipolar cycloaddition [J].

Artemov, A. N. ;

Sazonova, E. V. ;

Mavrina, E. A. ;

Zarovkina, N. Yu. .

RUSSIAN CHEMICAL BULLETIN, 2012, 61 (11) :2076-2081

[5] Metalated (η6-arene)tricarbonylchromium complexes in organometallic chemistry [J].

Berger, A ;

Djukic, JP ;

Michon, C .

COORDINATION CHEMISTRY REVIEWS, 2002, 225 (1-2) :215-238

[6] Arynes, diaryliodonium salts and azine N-oxides in transition metal-free electrophilic N-arylation [J].

Bugaenko, Dmitry I. ;

Karchava, Alexander V. ;

Yurovskaya, Marina A. .

RUSSIAN CHEMICAL REVIEWS, 2018, 87 (03) :272-301

[7] THE ANALYTICAL CALCULATION OF ABSORPTION IN MULTIFACETED CRYSTALS [J].

CLARK, RC ;

REID, JS .

ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 :887-897

[8]

Dotz K.H., 2004, METAL CARBENES ORGAN, P1

[9]

Farrugia L.J., 1999, J. Appl. Cryst, V32, P837, DOI [DOI 10.1107/S0021889899006020, 10.1107/S0021889812029111, DOI 10.1107/S0021889812029111]

[10] The QTAIM Approach to Chemical Bonding Between Transition Metals and Carbocyclic Rings: A Combined Experimental and Theoretical Study of (η5-C5H5)Mn(CO)3, (η6-C6H6)Cr(CO)3, and (E)-{(η5-C5H4)CF=CF(η5-C5H4)}(η5-C5H5)2Fe2 [J].

Farrugia, Louis J. ;

Evans, Cameron ;

Lentz, Dieter ;

Roemert, Max .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2009, 131 (03) :1251-1268

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