One-pot two-step stannylation/Stille homocoupling of aryl bromides and iodides under solvent-free conditions

被引：8

作者：

Gribanov, Pavel S. ^{[1
,2
]}

Golenko, Yulia D. ^{[1
]}

Topchiy, Maxim A. ^{[1
,2
]}

Philippova, Anna N. ^{[2
]}

Kirilenko, Nikita Yu. ^{[1
,2
]}

Krivoshchapov, Nikolai V. ^{[1
]}

Sterligov, Grigorii K. ^{[1
]}

Asachenko, Andrey F. ^{[1
,2
]}

Bermeshev, Maxim V. ^{[2
]}

Nechaev, Mikhail S. ^{[1
,2
]}

机构：

[1] Moscow MV Lomonosov State Univ, Dept Chem, Moscow 119991, Russia

[2] Russian Acad Sci, AV Topchiev Inst Petrochem Synth, Moscow 119991, Russia

来源：

MENDELEEV COMMUNICATIONS | 2018年 / 28卷 / 03期

基金：

俄罗斯科学基金会;

关键词：

CROSS-COUPLING REACTIONS; ENANTIOSELECTIVE SYNTHESIS; EFFICIENT SYNTHESIS; ALKENYL HALIDES; SOLAR-CELLS; PALLADIUM; COMPLEXES; SALTS; CHLORIDES; CATALYSTS;

D O I：

10.1016/j.mencom.2018.05.032

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A new highly efficient solvent-free method for aryl bromide (iodide) homocoupling comprising the use of Pd(OAc)(2)/PCy3 system in the presence of CsF is suitable for substrates bearing functional groups not tolerant to lithium-, magnesium-, zinc-organic reagents and strong bases.

引用

页码：323 / 325

页数：3

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