Synthesis of 3-(3-alkyl-5-thioxo-1H-4,5-dihydro-1,2,4-triazol-4-yl)aminocarbonylchromones

被引:0
作者
Cao, LH [1 ]
Zhang, L
Cui, PY
机构
[1] Xinjiang Univ, Coll Chem & Chem Engn, Urumqi 830046, Peoples R China
[2] Nankai Univ, State Key Lab Elementoorgan Chem, Tianjin 300071, Peoples R China
来源
KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII | 2004年 / 05期
关键词
3-(3-alkyl-5-thioxo-1H-4,5-dihydro-1,2,4-triazol-4-yl)aminocarbonylchromones; 3-formylchromone; synthesis;
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A series of 3-(3-alkyl-5-thioxo-1H-4,5-dihydro-1,2,4-triazol-4-yl)aminocarbonylchromones have been prepared by the oxidation of 3-formylchromone the Jones reagent followed by the reaction with 3-alkyl-4-amino-4,5-dihydro-1,2,4-triazole-5(1H)-thione in the presence Of POCl3. The structure of the compounds were confirmed by IR, LC-MS, H-1 NMR spectra and elemental analyses.
引用
收藏
页码:749 / 754
页数:6
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