Silicon and silicon carbide powders recycling technology from wire-saw cutting waste in slicing process of silicon ingots

被引:70
作者
Sergiienko, Sergii A. [1 ]
Pogorelov, Boris V. [2 ]
Daniliuk, Vladimir B. [3 ]
机构
[1] NASU, LV Pisarzhevsky Phys Chem Inst, UA-03028 Kiev, Ukraine
[2] NASU, V Bakul Inst Superhard Mat, UA-04074 Kiev, Ukraine
[3] NASU, Inst Electrodynam, UA-030680 Kiev, Ukraine
关键词
Solar cells; Wire-saw process; Silicon; Silicon carbide; SEPARATION PERFORMANCE; SLURRY;
D O I
10.1016/j.seppur.2014.06.036
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
A study on recycling silicon and silicon carbide powders from wire-saw slurry containing silicon carbide, silicon kerfs, polyethylene glycol (PEG), and iron fragments in the wire-saw slicing silicon ingots process was conducted. Recycling technology was suggested. PEG from the slurry was removed using filter press, and iron particles from the slurry were removed using high gradient magnetic separator. To separate silicon carbide and silicon particles hydrocyclone assembly was used. Recovered silicon carbide powder (95 wt% SiC, 4 wt% Si and 1 wt% Fe) can be used again in the process of cutting silicon ingots. Obtained recovered powder with high Si content after additional purification further can be used as a feedstock together with the amorphous silicon for crystal growth by directional solidification in an induction furnace. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:16 / 21
页数:6
相关论文
共 23 条
[1]  
Billiet R.L., 2004, U.S. patent, Patent No. [6780665, 6,780,665]
[2]  
Borisov V.G., 1968, REFRACT IND CERAM+, V9, P162
[3]   The role of Si-O species in the colloidal stability of silicon-containing ceramic powders [J].
Fukada, Y ;
Nicholson, PS .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2004, 24 (01) :17-23
[4]  
Horio M., 2003, U. S. Patent, Patent No. [6615817, 6,615,817]
[5]  
KAPUR VK, 1983, Patent No. 4388080
[6]   ADSORPTION OF METAL-IONS ON ACTIVATED CARBON FROM AQUEOUS-SOLUTIONS AT PH 1-13 [J].
KOSHIMA, H ;
ONISHI, H .
TALANTA, 1986, 33 (05) :391-395
[7]   Recovery of silicon powder from kerf loss slurry by centrifugation [J].
Lin, Yen-Chih ;
Wang, Teng-Yu ;
Lan, Chung-Wen ;
Tai, Clifford Y. .
POWDER TECHNOLOGY, 2010, 200 (03) :216-223
[8]  
Luque A., 2003, HDB PHOTOVOLTAIC SCI
[9]   Separation performance of sub-micron silica particles by electrical hydrocyclone [J].
Nenu, Romanus Krisantus Tue ;
Yoshida, Hideto ;
Fukui, Kunihiro ;
Yamamoto, Tetsuya .
POWDER TECHNOLOGY, 2009, 196 (02) :147-155
[10]  
Pizzini Sergio., 2012, Advanced Silicon Materials for Photovoltaic Applications, V1