Study of 'wet' polymer latex systems in environmental scanning electron microscopy: Some imaging considerations

被引:38
作者
Meredith, P
Donald, AM
机构
[1] Polymer and Colloids Group, University of Cambridge, Physics Department, Cambridge CB3 0HE, Madingley Road
来源
JOURNAL OF MICROSCOPY-OXFORD | 1996年 / 181卷
关键词
environmental scanning electron microscopy; polymer latex; contrast mechanisms;
D O I
10.1046/j.1365-2818.1996.67341.x
中图分类号
TH742 [显微镜];
学科分类号
摘要
Environmental scanning electron microscopy has been used to study 'wet' polymer latex films. Comparison of the results obtained by imaging in nitrogen and nitrous oxide gas and water vapour has provided insight into a variety of different contrast phenomena. Notably, it was found that edge definition and fine features could be enhanced by imposing further saturated vapour conditions at the hydrated film surface. Furthermore, by imaging at subzero temperatures in the presence of nitrogen, it was shown that beam damage could be reduced in such sensitive polymeric samples.
引用
收藏
页码:23 / 35
页数:13
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