Selective Synthesis of Cu2SnSe3 and Cu2SnSe4 Nanocrystals

被引：18

作者：

Ge, Zhen-Hua ^{[1
]}

Salvador, James R. ^{[2
]}

Nolas, George S. ^{[1
]}

机构：

[1] Univ S Florida, Dept Phys, Tampa, FL 33620 USA

[2] GM R&D Ctr, Chem & Mat Syst Lab, Warren, MI 48090 USA

来源：

INORGANIC CHEMISTRY | 2014年 / 53卷 / 09期

基金：

美国国家科学基金会;

关键词：

SOLVOTHERMAL SYNTHESIS; CRYSTAL-GROWTH; DIAMOND-LIKE; PHASE;

D O I：

10.1021/ic500100e

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The selective synthesis of Cu2SnSe3 and Cu2SnSe4 nanocrystals was achieved by a one-step solvothermal synthesis method. We also investigated the effects of different precursor sources and starting material concentrations on the phase purity of the products. Powder X-ray diffraction, elemental analysis, and magnetic susceptibility measurements were used to investigate the phase, purity, and homogeneity of the nanocrystals. This solvothermal approach is broadly applicable and may also be employed for the synthesis of other ternary or quaternary chalcogenide nanocrystals.

引用

页码：4445 / 4449

页数：5

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