Synthesis and characterization of flower-like MoO3/In2O3 microstructures for highly sensitive ethanol detection

被引:27
作者
Hu, Jie [1 ]
Wang, Xiu [1 ]
Zhang, Meng [1 ]
Sun, Yongjiao [1 ]
Li, Pengwei [1 ]
Zhang, Wendong [1 ]
Lian, Kun [1 ]
Chen, Lin [2 ]
Chen, Yong [3 ]
机构
[1] Taiyuan Univ Technol, Coll Informat Engn, Minist Educ,Micro & Nano Syst Res Ctr, Key Lab Adv Transducers & Intelligent Control Sys, Taiyuan 030024, Shanxi, Peoples R China
[2] Taiyuan Univ Technol, Res Ctr Adv Mat Sci & Technol, Taiyuan 030024, Shanxi, Peoples R China
[3] Ecole Normale Super, CNRS ENS UPMC UMR 8640, F-75005 Paris, France
基金
中国国家自然科学基金;
关键词
GAS-SENSING PERFORMANCE; ROOM-TEMPERATURE; IN2O3; SENSORS; OXIDES; SNO2; NO2; NANOSTRUCTURES; NANOSPHERES; FABRICATION;
D O I
10.1039/c7ra02593a
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Flower-like pure and Mo-loaded In2O3 hierarchical microstructures were synthesized by a facile hydrothermal method. The morphology, crystal structures, and compositions of the samples were characterized by SEM, XRD, TEM, showing nanosheets with dimensions of 4 mm diameter and 25 nm thickness. Gas sensing experiments were conducted on the as-prepared MoO3/In2O3 gas sensors, and the results prove that Mo-loaded In2O3 gas sensors exhibit enhanced gas sensing properties at 185 degrees C. In particular, the 3 mol% Mo-loaded In2O3 provided a high response (7 to 100 ppm ethanol), fast response and recovery time (11 s and 94 s), low detection limit (50 ppb), good selectivity and stability for ethanol detection, which is promising for low concentration ethanol detection in practical applications.
引用
收藏
页码:23478 / 23485
页数:8
相关论文
共 51 条
[1]   Enhanced ethanol sensing properties of multiple networked Au-doped In2O3 nanotube sensors [J].
An, Soyeon ;
Park, Sunghoon ;
Ko, Hyunsung ;
Jin, Changhyun ;
Lee, Wan In ;
Lee, Chongmu .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 2013, 74 (07) :979-984
[2]   WO3 nanorods/graphene nanocomposites for high-efficiency visible-light-driven photocatalysis and NO2 gas sensing [J].
An, Xiaoqiang ;
Yu, Jimmy C. ;
Wang, Yu ;
Hu, Yongming ;
Yu, Xuelian ;
Zhang, Guangjin .
JOURNAL OF MATERIALS CHEMISTRY, 2012, 22 (17) :8525-8531
[3]   CO gas sensing of CuO nanostructures, synthesized by an assisted solvothermal wet chemical route [J].
Aslani, Alireza ;
Oroojpour, Vahid .
PHYSICA B-CONDENSED MATTER, 2011, 406 (02) :144-149
[4]   Synthesis of porous In2O3 microspheres as a sensitive material for early warning of hydrocarbon explosions [J].
Cao, Yang ;
Zhao, Jun ;
Zou, Xiaoxin ;
Jin, Pan-Pan ;
Chen, Hui ;
Gao, Ruiqin ;
Zhou, Li-Jing ;
Zou, Yong-Cun ;
Li, Guo-Dong .
RSC ADVANCES, 2015, 5 (07) :5424-5431
[5]   A Single Eu-Doped In2O3 Nanobelt Device for Selective H2S Detection [J].
Chen, Weiwu ;
Liu, Yingkai ;
Qin, Zhaojun ;
Wu, Yuemei ;
Li, Shuanghui ;
Ai, Peng .
SENSORS, 2015, 15 (12) :29950-29957
[6]   Enhanced formaldehyde-sensing properties of mixed Fe2O3-In2O3 nanotubes [J].
Chi, Xiao ;
Liu, Changbai ;
Liu, Li ;
Li, Shouchun ;
Li, Haiying ;
Zhang, Xiaobo ;
Bo, Xiaoqing ;
Shan, Hao .
MATERIALS SCIENCE IN SEMICONDUCTOR PROCESSING, 2014, 18 :160-164
[7]   Trimethylamine sensing properties of sensors based on MoO3 microrods [J].
Chu, Xiangfeng ;
Liang, Shiming ;
Sun, Wenqi ;
Zhang, Wangbing ;
Chen, Tongyun ;
Zhang, Qianfeng .
SENSORS AND ACTUATORS B-CHEMICAL, 2010, 148 (02) :399-403
[8]  
Costello BPD, 2003, SENSOR ACTUAT B-CHEM, V92, P159, DOI 10.1016/SO925-4005(03)00258-2
[9]   Gas Sensing with Nano-Indium Oxides (In2O3) Prepared via Continuous Hydrothermal Flow Synthesis [J].
Elouali, Sofia ;
Bloor, Leanne G. ;
Binions, Russell ;
Parkin, Ivan P. ;
Carmalt, Claire J. ;
Darr, Jawwad A. .
LANGMUIR, 2012, 28 (03) :1879-1885
[10]   Influence of the Host Lattice Electronic Structure on Dilute Magnetic Interactions in Polymorphic Cr(III)-Doped In2O3 Nanocrystals [J].
Farvid, Shokouh S. ;
Hegde, Manu ;
Radovanovic, Pavle V. .
CHEMISTRY OF MATERIALS, 2013, 25 (02) :233-244