INFLUENCE OF CALCINATION PARAMETERS ON PHYSICOCHEMICAL AND STRUCTURAL PROPERTIES OF CO-PRECIPITATED MAGNESIUM SILICATE

被引:7
作者
Ciesielczyk, Filip [1 ]
Bartczak, Przemyslaw [1 ]
Klapiszewski, Lukasz [1 ]
Paukszta, Dominik [1 ]
Piasecki, Adam [2 ]
Jesionowski, Teofil [1 ]
机构
[1] Poznan Univ Tech, Fac Chem Technol, Inst Chem Technol & Engn, PL-60965 Poznan, Poland
[2] Poznan Univ Tech, Fac Mech Engn & Management, Inst Mat Sci & Engn, PL-60965 Poznan, Poland
来源
PHYSICOCHEMICAL PROBLEMS OF MINERAL PROCESSING | 2014年 / 50卷 / 01期
关键词
magnesium silicate; precipitation; calcination; WAXS; porous structure; PHOTOCATALYTIC ACTIVITY; OXIDE COMPOSITES; TEMPERATURE; SYSTEM;
D O I
10.5277/ppmp140111
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Physicochemical properties of different oxide systems depend mostly on the method of their preparation and classification, so the main aim of the study was to obtain the MgO center dot SiO2 hybrid in an aqueous solution and its calcination under assumed conditions. Research scope included evaluation of the effect of the basic parameters of the calcination process (time and temperature) on the structural properties of the final materials. Products obtained by the proposed method were thoroughly characterized. The chemical composition, crystalline structure, morphology and nature of the dispersion as well as parameters of the porous structure were established. The results of research in a decisive manner confirmed the possibility of designing the properties of inorganic oxide systems such as MgO center dot SiO2, which will definitively scheduled into potential directions for their use.
引用
收藏
页码:119 / 129
页数:11
相关论文
共 22 条
[1]   Precipitation of amorphous colloidal silica from aqueous solutions-Aggregation problem [J].
Baldyga, J. ;
Jasinska, M. ;
Jodko, K. ;
Petelski, P. .
CHEMICAL ENGINEERING SCIENCE, 2012, 77 :207-216
[2]   Synthesis and surfactant modification of clinoptilolite and montmorillonite for the removal of nitrate and preparation of slow release nitrogen fertilizer [J].
Bhardwaj, Deepesh ;
Sharma, Monika ;
Sharma, Pankaj ;
Tomar, Radha .
JOURNAL OF HAZARDOUS MATERIALS, 2012, 227 :292-300
[3]   Synthesis of mesoporous TiO2/γ-Al2O3 composite granules with different sol composition and calcination temperature [J].
Choi, Junseo ;
Kim, Jinsoo ;
Yoo, Kye Sang ;
Lee, Tai Gyu .
POWDER TECHNOLOGY, 2008, 181 (01) :83-88
[4]   Dispersive and electrokinetic evaluations of alkoxysilane-modified MgO•SiO2 oxide composite and pigment hybrids supported on it [J].
Ciesielczyk, Filip ;
Nowacka, Magdalena ;
Przybylska, Agnieszka ;
Jesionowski, Teofil .
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2011, 376 (1-3) :21-30
[5]   Calcined sodium silicate as solid base catalyst for biodiesel production [J].
Guo, Feng ;
Peng, Zhen-Gang ;
Dai, Jian-Ying ;
Xiu, Zhi-Long .
FUEL PROCESSING TECHNOLOGY, 2010, 91 (03) :322-328
[6]   HEAT TREATMENT OF NATURAL DIATOMITE [J].
Ibrahim, Suzan S. ;
Selim, Ali Q. .
PHYSICOCHEMICAL PROBLEMS OF MINERAL PROCESSING, 2012, 48 (02) :413-424
[7]   Nano-structured silicas and silicates - new materials and their applications in paper [J].
Johnston, JH ;
McFarlane, AJ ;
Borrmann, T ;
Moraes, J .
CURRENT APPLIED PHYSICS, 2004, 4 (2-4) :411-414
[8]   Influence of calcination temperature on structural and optical properties of TiO2 thin films prepared by sol-gel dip coating [J].
Kim, DJ ;
Hahn, SH ;
Oh, SH ;
Kim, EJ .
MATERIALS LETTERS, 2002, 57 (02) :355-360
[9]  
Laurentowska A, 2012, PHYSICOCHEM PROBL MI, V48, P63
[10]   Effects of sodium content and calcination temperature on the morphology, structure and photocatalytic activity of nanotubular titanates [J].
Lee, Chung-Kung ;
Wang, Cheng-Cai ;
Lyu, Meng-Du ;
Juang, Lain-Chuen ;
Liu, Shin-Shou ;
Hung, Shui-Hung .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2007, 316 (02) :562-569