Influence of heat treatment medium on properties of the bovine hydroxyapatite/magnetite systems

被引:0
作者
Otychenko, Oksana [1 ]
Babutina, Tetyana [1 ]
Perekos, Anatolii [2 ]
Bykov, Oleksandr [3 ]
Korichev, Sergiy [3 ]
Koval, Oleksandr [4 ]
机构
[1] NAS Ukraine, Dept Funct Mat Med Applicat, Frantsevich Inst Problems Mat Sci, 3 Krzhizhanovsky Str, UA-03142 Kiev, Ukraine
[2] NAS Ukraine, Kurdyumov Inst Met Phys, Dept Constitut & Properties Solid Solut, 36 Academician Vernadsky Blvd, UA-03142 Kiev, Ukraine
[3] NAS Ukraine, Frantsevich Inst Problems Mat Sci, Dept Phys Mat Sci Refractory Cpds, 3 Krzhizhanovsky Str, UA-03142 Kiev, Ukraine
[4] NAS Ukraine, Frantsevich Inst Problems Mat Sci, Dept Phys Strength & Plast Mat, 3 Krzhizhanovsky Str, UA-03142 Kiev, Ukraine
来源
MATERIA-RIO DE JANEIRO | 2020年 / 25卷 / 04期
基金
中国国家自然科学基金;
关键词
bovine hydroxyapatite; magnetite; crystallinity; specific saturation magnetization; in vitro experiments; SPECTROSCOPIC CHARACTERIZATION; MAGNETIC HYDROXYAPATITE; BIOGENIC HYDROXYAPATITE; NANOPARTICLES;
D O I
10.1590/S1517-707620200004.1174
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Technological processes for the synthesis of composite systems based on bovine (rather than synthetic) hydroxyapatite are rarely described. That's why the influence of the heat treatment medium on the properties of the composite system bovine hydroxyapatite/magnetite (BHA/Fe3O4) obtained using physico-mechanical and chemical methods were investigated. It was established that the most efficient medium for heat treatment of studied materials is vacuum. Due to XRD analysis data allow us to assert that the most perfect lattice is formed with the use of the chemical method for production and heat treatment in a vacuum (crystallinity 86%), and the least perfect one is formed by the mechanical method for production and heat treatment in a nitrogen medium (71%). The method for adding magnetite has only a minor effect. Investigated conditions of heat treatment of composite systems BHA/Fe3O4 promoted obtaining optimal magnetic properties and stable behavior in experiments in vitro.
引用
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页码:1 / 13
页数:13
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