Solvent-free route to ionic liquid precursors using a water-moderated microwave process

被引:65
作者
Law, MC
Wong, KY
Chan, TH [1 ]
机构
[1] Hong Kong Polytech Univ, Dept Appl Biol & Chem Technol, Hong Kong, Hong Kong, Peoples R China
[2] Hong Kong Polytech Univ, Inst Mol Technol Drug Discovery & Synth, Open Lab Chiral Technol, Hong Kong, Hong Kong, Peoples R China
关键词
D O I
10.1039/b203122a
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Water moderation has been used for solvent-free microwave assisted reactions which generate over-heating. The method is demonstrated by the large scale preparation of ionic liquid precursors.
引用
收藏
页码:328 / 330
页数:3
相关论文
共 32 条
  • [11] Ionic liquid-polymer gel electrolytes from hydrophilic and hydrophobic ionic liquids
    Fuller, J
    Breda, AC
    Carlin, RT
    [J]. JOURNAL OF ELECTROANALYTICAL CHEMISTRY, 1998, 459 (01): : 29 - 34
  • [12] The room temperature ionic liquid 1-ethyl-3-methylimidazolium tetrafluoroborate: Electrochemical couples and physical properties
    Fuller, J
    Carlin, RT
    Osteryoung, RA
    [J]. JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1997, 144 (11) : 3881 - 3886
  • [13] A simple colorimetric method for the quality control of 1-alkyl-3-methylimidazolium ionic liquid precursors
    Holbrey, JD
    Seddon, KR
    Wareing, R
    [J]. GREEN CHEMISTRY, 2001, 3 (01) : 33 - 36
  • [14] Moisture stable ambient temperature ionic liquids: Solvents for the new millennium. 1. The heck reaction
    Howarth, J
    Dallas, A
    [J]. MOLECULES, 2000, 5 (06): : 851 - 855
  • [15] Room temperature ionic liquids as novel media for 'clean' liquid-liquid extraction
    Huddleston, JG
    Willauer, HD
    Swatloski, RP
    Visser, AE
    Rogers, RD
    [J]. CHEMICAL COMMUNICATIONS, 1998, (16) : 1765 - 1766
  • [16] The synthesis and reaction of zinc reagents in ionic liquids
    Kitazume, T
    Kasai, K
    [J]. GREEN CHEMISTRY, 2001, 3 (01) : 30 - 32
  • [17] KOEL M, 2000, P ESTONIAN ACAD SCI, V493, P145
  • [18] Highly diastereoselective synthesis of 1,3-oxazolidines under thermodynamic control using focused microwave irradiation under solvent-free conditions
    Kuhnert, N
    Danks, TN
    [J]. GREEN CHEMISTRY, 2001, 3 (02) : 68 - 70
  • [19] Kumar HMS, 1999, GREEN CHEM, V1, P141
  • [20] Metal mediated allylation of carbonyl compounds in ionic liquids
    Law, MC
    Wong, KY
    Chan, TH
    [J]. GREEN CHEMISTRY, 2002, 4 (02) : 161 - 164