Synthesis, optical and morphological characterization of MPA-capped PbSe nanocrystals

被引:2
|
作者
Ouma, Immaculate L. A. [1 ]
Mushonga, Paul [1 ]
Madiehe, Abram M. [2 ]
Meyer, Mervin [2 ]
Dejene, Francis B. [3 ]
Onani, Martin O. [1 ]
机构
[1] Univ Western Cape, Dept Chem, ZA-7535 Bellville, South Africa
[2] Univ Western Cape, Dept Biotechnol, ZA-7535 Bellville, South Africa
[3] Univ Free State, Dept Phys, ZA-9866 Phuthaditjhaba, South Africa
关键词
Nanocrystals (NCs); PbSe; Near-infrared (NIR); 3-mercaptopropionic acid (MPA); QUANTUM DOTS; SEMICONDUCTOR NANOCRYSTALS; AQUEOUS-SOLUTION;
D O I
10.1016/j.physb.2013.10.057
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
This work focuses on the synthesis and characterization of 3-mercaptopropionic acid capped PbSe nanocrystals (NCs) using an aqueous synthetic protocol. The synthesis was carried out at room temperature and resulted in uniform NCs. The as synthesized NCs were characterized using photoluminescence spectroscopy, HR-TEM and X-Ray diffraction. They showed a perfect Gaussian peak at 1203 urn with average diameters of <= 3 nm and diffraction patterns consistent with rock salt structure of PbSe NCs. (C) 2013 Elsevier B.V. All rights reserved.
引用
收藏
页码:130 / 132
页数:3
相关论文
共 50 条
  • [21] Structural and Optical Properties of Co2+-Doped PbSe Nanocrystals in Chalcogeneide Glass Matrix
    Lourenco, Sidney A.
    Silva, Ricardo S.
    Silva, A. C. A.
    Dantas, Noelio O.
    JOURNAL OF PHYSICAL CHEMISTRY C, 2015, 119 (23) : 13277 - 13282
  • [22] A Facile Phosphine-Free Method for Synthesizing PbSe Nanocrystals with Strong Optical Limiting Effects
    Wang, Tian-Ming
    Gao, Bao
    Wang, Qiang
    Zhao, Min
    Kang, Kai-Bin
    Xu, Zhu-Guo
    Zhang, Hao-Li
    CHEMISTRY-AN ASIAN JOURNAL, 2013, 8 (05) : 912 - 918
  • [23] Characterization of CdTe nanocrystals during their synthesis in liquid paraffin: optical properties and particle growth
    Yordanov, Georgi
    Yoshimura, Hideyuki
    Dushkin, Ceco
    JOURNAL OF MATERIALS SCIENCE, 2011, 46 (07) : 2338 - 2344
  • [24] Effect of hydrazine hydrate on the luminescence properties of MPA capped CdTe nanocrystals in hot injection method
    Mobedi, N.
    Marandi, M.
    Bidaki, H. Zare
    JOURNAL OF LUMINESCENCE, 2014, 156 : 235 - 239
  • [25] Synthesis, characterization and stability study of aqueous MPA capped CuInS2/ZnS core/shell nanoparticles
    Jain, Shikshita
    Bharti, Shivani
    Bhullar, Gurvir Kaur
    Tripathi, S. K.
    JOURNAL OF LUMINESCENCE, 2022, 252
  • [26] Optical investigation of quantum confinement in PbSe nanocrystals at different points in the Brillouin zone
    Koole, Rolf
    Allan, Guy
    Delerue, Christophe
    Meijerink, Andries
    Vanmaekelbergh, Daniel
    Houtepen, Arjan J.
    SMALL, 2008, 4 (01) : 127 - 133
  • [27] Study of the aqueous synthesis, optical and electrochemical characterization of alloyed ZnxCd1-xTe nanocrystals
    Santos Matos, Charlene Regina
    Candido, Luan P. M.
    Souza, Helio Oliveira, Jr.
    da Costa, Luiz Pereira
    Sussuchi, Eliana Midori
    Gimenez, Iara F.
    MATERIALS CHEMISTRY AND PHYSICS, 2016, 178 : 104 - 111
  • [28] Enzyme mediated synthesis of phytochelatin-capped CdS nanocrystals
    Liu, Fang
    Kang, Seung Hyun
    Lee, Young-In
    Choa, Yong-ho
    Mulchandani, Ashok
    Myung, Nosang V.
    Chen, Wilfred
    APPLIED PHYSICS LETTERS, 2010, 97 (12)
  • [29] Synthesis, optical and morphological characterization of doped InP/ZnSe NCs
    Mushonga, Paul
    Ouma, Immaculate L. A.
    Madiehe, Abram M.
    Meyer, Mervin
    Dejene, Francis B.
    Onani, Martin O.
    PHYSICA B-CONDENSED MATTER, 2014, 439 : 189 - 192
  • [30] Synthesis and Ligand Exchange of Thiol-Capped Silicon Nanocrystals
    Yu, Yixuan
    Rowland, Clare E.
    Schaller, Richard D.
    Korgel, Brian A.
    LANGMUIR, 2015, 31 (24) : 6886 - 6893