Synthesis of magnetite nanoparticles for AC magnetic heating

被引:63
作者
Hosono, T. [1 ]
Takahashi, H. [1 ]
Fujita, A. [2 ]
Joseyphus, R. Justin [1 ,3 ]
Tohji, K. [1 ]
Jeyadevan, B. [1 ]
机构
[1] Tohoku Univ, Grad Sch Environm Studies, Aoba Ku, Sendai, Miyagi 9808579, Japan
[2] Tohoku Univ, Grad Sch Engn, Aoba Ku, Sendai, Miyagi 9808579, Japan
[3] Natl Inst Technol, Dept Phys, Tiruchirappalli 620015, Tamil Nadu, India
关键词
pH-stabilized; Coprecipitation; Magnetic hyperthermia; Magnetite; AC heating; HYPERTHERMIA; PARTICLES;
D O I
10.1016/j.jmmm.2009.04.061
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Magnetite particles with different average diameter (D-m) suitable for magnetic fluid hyperthermia (MFH) were synthesized by controlled coprecipitation technique. In this method, the reaction pH was stabilized using the pH buffer and the average particle diameter decreased with increasing reaction pH. The size-dependent magnetic behaviour of the magnetite nanoparticles was studied and the optimum size range required for magnetic fluid hyperthermia (MFH) has been arrived at. Among the samples studied, the maximum specific absorption rate of 15.7 W/g was recorded for the magnetite sample with D-m of 13 nm, when exposed to an AC magnetic field strength of 3.2 kA/m and frequency of 600 kHz. The AC magnetic properties suggested that the size distribution of the sample was bimodal with average particle size less than similar to 13 nm. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:3019 / 3023
页数:5
相关论文
共 13 条
[1]  
Atsumi T., 2006, Journal of the Magnetics Society of Japan, V30, P555, DOI 10.3379/jmsjmag.30.555
[2]  
ATSUMI T, 2006, THESIS TOHOKU U JAPA
[3]   Heating efficiency of magnetite particles exposed to AC magnetic field [J].
Atsumi, Takashi ;
Jeyadevan, Balachandran ;
Sato, Yoshinori ;
Tohji, Kazuyuki .
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2007, 310 (02) :2841-2843
[4]   Maghemite nanoparticles with very high AC-losses for application in RF-magnetic hyperthermia [J].
Hergt, R ;
Hiergeist, R ;
Hilger, I ;
Kaiser, WA ;
Lapatnikov, Y ;
Margel, S ;
Richter, U .
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2004, 270 (03) :345-357
[5]   Physical limits of hyperthermia using magnetite fine particles [J].
Hergt, R ;
Andra, W ;
d'Ambly, CG ;
Hilger, I ;
Kaiser, WA ;
Richter, U ;
Schmidt, HG .
IEEE TRANSACTIONS ON MAGNETICS, 1998, 34 (05) :3745-3754
[6]  
Hosono T, 2007, AIP CONF PROC, V898, P135, DOI 10.1063/1.2721264
[7]   Clinical hyperthermia of prostate cancer using magnetic nanoparticles:: Presentation of a new interstitial technique [J].
Johannsen, M ;
Gneveckow, U ;
Eckelt, L ;
Feussner, A ;
Waldöfner, N ;
Scholz, R ;
Deger, S ;
Wust, P ;
Loening, SA ;
Jordan, A .
INTERNATIONAL JOURNAL OF HYPERTHERMIA, 2005, 21 (07) :637-647
[8]   Protective coating of superparamagnetic iron oxide nanoparticles [J].
Kim, DK ;
Mikhaylova, M ;
Zhang, Y ;
Muhammed, M .
CHEMISTRY OF MATERIALS, 2003, 15 (08) :1617-1627
[9]   MEASUREMENTS OF THE ANISOTROPY CONSTANT IN NI-FE AND FE3O4 MAGNETIC FLUIDS [J].
LAMBRICK, DB ;
HOON, SR ;
MASON, N ;
KILNER, M .
IEEE TRANSACTIONS ON MAGNETICS, 1988, 24 (02) :1647-1649
[10]   Superparamagnetism of magnetite nanoparticles: Dependence on surface modification [J].
Mikhaylova, M ;
Kim, DK ;
Bobrysheva, N ;
Osmolowsky, M ;
Semenov, V ;
Tsakalakos, T ;
Muhammed, M .
LANGMUIR, 2004, 20 (06) :2472-2477