Reference and normalization methods: Essential tools for the intercomparison of NMR spectra

被引：55
作者：
Giraudeau, Patrick [1 ]
Tea, Illa [1 ]
Remaud, Gerald S. [1 ]
Akoka, Serge [1 ]
机构：
[1] Univ Nantes, LUNAM Univ, CNRS, EBSI Team,Modelisat CEISAM,UMR 6230, F-44322 Nantes 03, France
来源：
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS | 2014年 / 93卷
关键词：
qNMR; Quantitative NMR spectroscopy; NMR spectrometry; Chemical reference; Electronic reference; HR-MAS SPECTROSCOPY; SOLID-STATE NMR; QUANTITATIVE NMR; PROTON NMR; 2D NMR; ABSOLUTE QUANTIFICATION; ERETIC METHOD; METABOLITE CONCENTRATIONS; INTERNAL STANDARD; LACTIC-ACID;
D O I：
10.1016/j.jpba.2013.07.020
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
This review aims at providing an analysis of the various available reference methods in nuclear magnetic resonance, based on recent literature. This paper will provide a tool to help users in choosing the appropriate method depending on the NMR experiment, sample and targeted application. For each method, the crucial parameters that should be particularly considered to reach the accuracy objectives of quantitative NMR are described. After defining the main concepts, the principle, the analytical performance and the main recent applications of each method are described, and a critical discussion is finally provided. (C) 2013 Elsevier B.V. All rights reserved.
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页码：3 / 16
页数：14
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