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Crystal structure of 4-(2-hydroxy-3-methoxy-benzylamino)benzoic acid dimethylformamide monosolvate monohydrate
被引:0
作者:
Faizi, Md Serajul Haque
[1
]
Kamaal, Saima
[2
]
Ali, Arif
[2
]
Ahmad, Musheer
[2
]
Golenya, Irina A.
[3
]
机构:
[1] BRA Bihar Univ, Langat Singh Coll, Dept Chem, Muzaffarpur 842001, Bihar, India
[2] Aligarh Muslim Univ, Fac Engn & Technol, Dept Appl Chem, Aligarh 202002, Uttar Pradesh, India
[3] Natl Taras Shevchenko Univ, Dept Chem, Volodymyrska Str 64, UA-01601 Kiev, Ukraine
关键词:
crystal structure;
2-hydroxy-3-methoxy-benzaldehyde;
4-aminobenzoic acid (PABA);
secondary amine;
hydrogen bonding;
vanillin derivative;
dimethylformamide solvate;
D O I:
10.1107/S2056989019005103
中图分类号:
O7 [晶体学];
学科分类号:
0702 ;
070205 ;
0703 ;
080501 ;
摘要:
The title compound, C15H15NO4 center dot C3H7NO center dot H2O, a secondary amine molecule, is accompanied by one equivalent of water and one equivalent of dimethylformamide (DMF) as solvents. The molecule is non-planar, with a C-aryl-CH2-NH-C-aryl torsion angle of -66.3 (3)degrees. In the crystal, O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen-bonding interactions between the amine molecules and the two types of solvent molecule result in the formation of a layered structure extending parallel to (010).
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页码:646 / +
页数:9
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