Crystal structure of 4-(2-hydroxy-3-methoxy-benzylamino)benzoic acid dimethylformamide monosolvate monohydrate

被引：0

作者：

Faizi, Md Serajul Haque ^{[1
]}

Kamaal, Saima ^{[2
]}

Ali, Arif ^{[2
]}

Ahmad, Musheer ^{[2
]}

Golenya, Irina A. ^{[3
]}

机构：

[1] BRA Bihar Univ, Langat Singh Coll, Dept Chem, Muzaffarpur 842001, Bihar, India

[2] Aligarh Muslim Univ, Fac Engn & Technol, Dept Appl Chem, Aligarh 202002, Uttar Pradesh, India

[3] Natl Taras Shevchenko Univ, Dept Chem, Volodymyrska Str 64, UA-01601 Kiev, Ukraine

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2019年 / 75卷

关键词：

crystal structure; 2-hydroxy-3-methoxy-benzaldehyde; 4-aminobenzoic acid (PABA); secondary amine; hydrogen bonding; vanillin derivative; dimethylformamide solvate;

D O I：

10.1107/S2056989019005103

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C15H15NO4 center dot C3H7NO center dot H2O, a secondary amine molecule, is accompanied by one equivalent of water and one equivalent of dimethylformamide (DMF) as solvents. The molecule is non-planar, with a C-aryl-CH2-NH-C-aryl torsion angle of -66.3 (3)degrees. In the crystal, O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen-bonding interactions between the amine molecules and the two types of solvent molecule result in the formation of a layered structure extending parallel to (010).

引用

页码：646 / +

页数：9

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