Preparation and Adsorption Capacity of Flower-Like Magnesium Oxide

被引:1
作者
Cheng Wen-Ting [1 ]
Chen Ya-Fen [1 ]
Li Yang [2 ]
Cheng Fang-Qin [1 ]
机构
[1] Shanxi Univ, Inst Resources & Environm Engn, State Environm Protect Key Lab Efficient Resource, Taiyuan 030006, Peoples R China
[2] Beijing Univ Chem Technol, State Key Lab Chem Resource Engn, Beijing 100029, Peoples R China
关键词
flower-like MgO; basic magnesium carbonate; CTAB; citric acid method; adsorption capacity; FT-IR ANALYSIS; CARBONATE; DECOMPOSITION; KINETICS; MGO;
D O I
10.3969/j.issn.1001-4861.2013.00.250
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
A novel adsorbent of flower-like magnesium oxide has been prepared via hydrothermal method using CTAB as a structure director. Experiment results showed that the precursor of flower-like MgO is basic magnesium carbonate, and MgO with large surface area was obtained after calcination at 600 degrees C. The adsorption performance of flower-like MgO was also studied in lead solution. The results of adsorption are conformed to Langmuir model, and maximum adsorption is 320 mg.g(-1), which means the novel flower-like MgO has a high adsorption performance.
引用
收藏
页码:1793 / 1798
页数:6
相关论文
共 42 条
[1]   Synthesis of micrometer-sized nanostructured magnesium oxide and its high catalytic activity in the Claisen-Schmidt condensation reaction (vol 112C, pg 11340, 2008) [J].
Bian, Shao-Wei ;
Ma, Zhuo ;
Cui, Zhi-Min ;
Zhang, Le-Sheng ;
Niu, Fang ;
Song, Wei-Guo .
JOURNAL OF PHYSICAL CHEMISTRY C, 2008, 112 (39) :15602-15602
[2]   DTA and FT-IR analysis of the rehydration of basic magnesium carbonate [J].
Botha, A ;
Strydom, CA .
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2003, 71 (03) :987-995
[3]   Preparation of a magnesium hydroxy carbonate from magnesium hydroxide [J].
Botha, A ;
Strydom, CA .
HYDROMETALLURGY, 2001, 62 (03) :175-183
[4]   Superb Adsorption Capacity and Mechanism of Flowerlike Magnesium Oxide Nanostructures for Lead and Cadmium Ions [J].
Cao, Chang-Yan ;
Qu, Jin ;
Wei, Fang ;
Liu, Hua ;
Song, Wei-Guo .
ACS APPLIED MATERIALS & INTERFACES, 2012, 4 (08) :4283-4287
[5]   Nucleation kinetics of nesquehonite (MgCO3 • 3H2O) in the MgCl2-Na2CO3 system [J].
Cheng, Wenting ;
Li, Zhibao .
JOURNAL OF CRYSTAL GROWTH, 2010, 312 (09) :1563-1571
[6]   Controlled Supersaturation Precipitation of Hydromagnesite for the MgCl2-Na2CO3 System at Elevated Temperatures: Chemical Modeling and Experiment [J].
Cheng, Wenting ;
Li, Zhibao .
INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 2010, 49 (04) :1964-1974
[7]   Synthesis of flavanones using nanocrystalline MgO [J].
Choudary, BM ;
Ranganath, KVS ;
Yadav, J ;
Kantam, ML .
TETRAHEDRON LETTERS, 2005, 46 (08) :1369-1371
[8]   INFLUENCE OF PREPARATION CONDITIONS OF BASIC MAGNESIUM CARBONATE ON ITS THERMAL-ANALYSIS [J].
CHOUDHARY, VR ;
PATASKAR, SG ;
GUNJIKAR, VG ;
ZOPE, GB .
THERMOCHIMICA ACTA, 1994, 232 (01) :95-110
[9]   Kinetics of heterogeneously MgO-catalyzed transesterification [J].
Dossin, TF ;
Reyniers, MF ;
Marin, GB .
APPLIED CATALYSIS B-ENVIRONMENTAL, 2006, 62 (1-2) :35-45
[10]   Emulsion-phase synthesis of honeycomb-like Mg5(OH)2(CO3)4•4H2O micro-spheres and subsequent decomposition to MgO [J].
Gao, Guo ;
Xiang, Lan .
JOURNAL OF ALLOYS AND COMPOUNDS, 2010, 495 (01) :242-246