Characterization of Ni-Fe/Si3N4 Nanocomposite Coatings Deposited by Electroplating

被引:0
作者
Marita, Yusrini [1 ]
Yaacob, Iskandar Idris [1 ]
机构
[1] Univ Malaya, Ctr Nanotechnol Precis & Adv Mat, Kuala Lumpur 50603, Malaysia
来源
CURRENT THEMES IN ENGINEERING SCIENCE 2008 | 2009年 / 1138卷
关键词
Electroplating; Nanocomposite; Ni-Fe- Si(3)N(4); Si(3)N(4) nano-particulates; COMPOSITE COATINGS; FILMS; ELECTRODEPOSITION; PARTICLES; DC;
D O I
暂无
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Ni-Fe/Si(3)N(4) nanocomposite coatings with various amount of Si(3)N(4) were prepared by electrodeposition technique. The effect of Si(3)N(4) nanoparticulatcs in the Ni-Fe nanocomposite coatings was investigated in relation to the ratio of Si(3)N(4) to Na-saccharine in the plating bath. X-ray diffraction analysis showed that the Ni-Fe nanocomposite coating has face-centered cubic structure (FCC). However, a mixture of body-centered cubic (BCC) and face-centered cubic (FCC) phases was observed when the ratio of Si(3)N(4) to Na-saccharine was around 8.3. The crystallite size of the Ni-Fe nanocomposite coating decreased when the ratio of Si(3)N(4) to Na-saccharine was increased. From the results of the elemental mapping procedure, it was found that inclusions of silicon were uniformly distributed in Ni-Fe composite coating, indicating good dispersion of Si(3)N(4) and this contributed in increasing the microhardness of coating.
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页码:106 / 116
页数:11
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