A Simple Device for Lens-to-Sample Distance Adjustment in Laser-Induced Breakdown Spectroscopy (LIBS)

被引:22
作者
Cortez, Juliana [1 ]
Farias Filho, Benedito B. [1 ]
Fontes, Laiane M. [1 ]
Pasquini, Celio [1 ]
Raimundo, Ivo M., Jr. [1 ]
Pimentel, Maria Fernanda [2 ]
Lins Borba, Flavia de Souza [3 ]
机构
[1] Univ Estadual Campinas, Dept Analyt Chem, Chem Inst, Campinas, SP, Brazil
[2] Univ Fed Pernambuco, Dept Chem Engn, Recife, PE, Brazil
[3] Univ Fed Pernambuco, Dept Fundamental Chem, Recife, PE, Brazil
基金
巴西圣保罗研究基金会;
关键词
Laser-induced breakdown spectroscopy; LIBS; lens-to-sample distance; sample positioning; repeatability;
D O I
10.1177/0003702816687571
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A simple device based on two commercial laser pointers is described to assist in the analysis of samples that present uneven surfaces and/or irregular shapes using laser-induced breakdown spectroscopy (LIBS). The device allows for easy positioning of the sample surface at a reproducible distance from the focusing lens that conveys the laser pulse to generate the micro-plasma in a LIBS system, with reproducibility better than +/- 0.2 mm. In this way, fluctuations in the fluence (J cm(-2)) are minimized and the LIBS analytical signals can be obtained with a better precision even when samples with irregular surfaces are probed.
引用
收藏
页码:634 / 639
页数:6
相关论文
共 16 条
[1]  
[Anonymous], 2006, Handbook of Laser-Induced Breakdown Spectroscopy
[2]   Repeatability improvement of laser-induced breakdown spectroscopy using an auto-focus system [J].
Ashrafkhani, Behnam ;
Bahreini, Maryam ;
Tavassoli, Seyed Hassan .
OPTICS AND SPECTROSCOPY, 2015, 118 (05) :841-846
[3]  
Borba FDL, 2012, J BRAZIL CHEM SOC, V23, P958, DOI 10.1590/S0103-50532012000500023
[4]   Pigment analysis in Bronze Age Aegean and Eastern Mediterranean painted plaster by laser-induced breakdown spectroscopy (LIBS) [J].
Brysbaert, Ann ;
Melessanaki, Krystalia ;
Anglos, Demetrios .
JOURNAL OF ARCHAEOLOGICAL SCIENCE, 2006, 33 (08) :1095-1104
[5]   Characterization of Iron age pottery from eastern Turkey by laser-induced breakdown spectroscopy (LIBS) [J].
Erdem, A. ;
Cilingiroglu, A. ;
Giakoumaki, A. ;
Castanys, M. ;
Kartsonaki, E. ;
Fotakis, C. ;
Anglos, D. .
JOURNAL OF ARCHAEOLOGICAL SCIENCE, 2008, 35 (09) :2486-2494
[6]   Laser-induced breakdown spectroscopy (LIBS) in archaeological science-applications and prospects [J].
Giakoumaki, Anastasia ;
Melessanaki, Kristalia ;
Anglos, Demetrios .
ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2007, 387 (03) :749-760
[7]   Compositional analysis of Hispanic Terra Sigillata by laser-induced breakdown spectroscopy [J].
López, AJ ;
Nicolás, G ;
Mateo, MP ;
Piñón, V ;
Tobar, MJ ;
Ramil, A .
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 2005, 60 (7-8) :1149-1154
[8]   The application of LIBS for the analysis of archaeological ceramic and metal artifacts [J].
Melessanaki, K ;
Mateo, M ;
Ferrence, SC ;
Betancourt, PP ;
Anglos, D .
APPLIED SURFACE SCIENCE, 2002, 197 :156-163
[9]   Review: Applications of single-shot laser-induced breakdown spectroscopy [J].
Michel, Anna P. M. .
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 2010, 65 (03) :185-191
[10]   Precise alignment of the collection fiber assisted by real-time plasma imaging in laser-induced breakdown spectroscopy [J].
Motto-Ros, V. ;
Negre, E. ;
Pelascini, F. ;
Panczer, G. ;
Yu, J. .
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 2014, 92 :60-69