Biopolymer-assisted green synthesis and characterization of calcium hydroxide nanoparticles

被引:52
作者
Darroudi, Majid [1 ,2 ]
Bagherpour, Maryam [3 ,4 ]
Hosseini, Hasan Ali [5 ]
Ebrahimi, Mahmoud [3 ]
机构
[1] Mashhad Univ Med Sci, Sch Med, Nucl Med Res Ctr, Mashhad, Iran
[2] Mashhad Univ Med Sci, Sch Med, Dept Modern Sci & Technol, Mashhad, Iran
[3] Islamic Azad Univ, Mashhad Branch, Dept Chem, Mashhad 917751436, Iran
[4] Astan Qods Razavi Museum & Lib, Conservator Cultural Heritage, Mashhad, Iran
[5] Payame Noor Univ, Dept Chem, Tehran 193954697, Iran
关键词
Calcium hydroxide; Nanoparticles; Biopolymer; Gelatin; Powder X-ray diffraction; CULTURAL-HERITAGE CONSERVATION; CA(OH)(2) NANOPARTICLES; OXIDE NANOPARTICLES; DEACIDIFICATION; CONSOLIDATION; NANOCERIA;
D O I
10.1016/j.ceramint.2015.11.045
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The use of biopolymers in the synthesis of different nanostructures can be a cost effective and eco-friendly approach. In the present study, a facile and "green" sol gel method was employed for preparing calcium hydroxide nanoparticles (Ca(OH)(2)-NPs) in gelatin matrix as a bio-template. Prepared nanoparticles were characterized by different instruments such as powder X-ray diffraction (PXRD), field emission scanning electron microscopy (EBSEM), and Fourier transform infrared spectroscopy (FTIR). The PXRD analysis revealed hexagonal Ca(OH)(2)-NPs with preferential orientation in (101) reflection plane. They are hexagonal in shape with a mean particle size of approximately 42 nm in thickness. The synthesized Ca(OH)(2)-NPs using gelatin were found to be comparable to those obtained from conventional methods using hazardous capping/stabilizing polymeric agents or surfactants and this route can be an excellent alternative for the synthesis of Ca(OH)(2)-NPs using biomaterials. (C) 2015 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:3816 / 3819
页数:4
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