Synthesis of manganese dioxide by homogeneous hydrolysis in the presence of melamine

被引：4

作者：

Sharipov, Kh. B. ^{[1
]}

Yapryntsev, A. D. ^{[2
]}

Baranchikov, A. E. ^{[2
]}

Boytsova, O. V. ^{[1
,2
]}

Kurzeev, S. A. ^{[1
]}

Ivanova, O. S. ^{[2
]}

Borilo, L. P. ^{[3
]}

Gil'mutdinov, F. Z. ^{[4
]}

Kozik, V. V. ^{[3
]}

Ivanov, V. K. ^{[2
,3
]}

机构：

[1] Moscow MV Lomonosov State Univ, Moscow 119991, Russia

[2] Russian Acad Sci, Kurnakov Inst Gen & Inorgan Chem, Moscow 119991, Russia

[3] Tomsk State Univ, Tomsk 634050, Russia

[4] Russian Acad Sci, Phys Tech Inst, Ural Branch, Izhevsk 426000, Russia

来源：

RUSSIAN JOURNAL OF INORGANIC CHEMISTRY | 2017年 / 62卷 / 02期

基金：

俄罗斯基础研究基金会;

关键词：

nanocrystalline manganese dioxide; potassium permanganate; melamine; hydrothermal microwave treatment; selective synthesis of MnO2 polymorphs; ASSISTED HYDROTHERMAL SYNTHESIS; PHASE-TRANSFORMATION; STRUCTURAL DEFECTS; OXIDES; PRECIPITATION; CRYPTOMELANE; BIRNESSITE; GAMMA-MNO2; NITRATE;

D O I：

10.1134/S0036023617020164

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A new selective method for the synthesis of nanocrystalline manganese dioxide (alpha-, beta-, and gamma-MnO2) based on the reaction of potassium permanganate with 2,4,6-triamino-1,3,5-triazine (melamine) under hydrothermal conditions has been proposed. Effect of synthesis conditions on the phase composition of the products has been revealed. A new manganese-containing phase with layered structure has been prepared.

引用

页码：139 / 149

页数：11

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