Impact of 1-Methylimidazole on Crystal Formation, Phase Transitions, and Glass Formation in a Zeolitic Imidazolate Framework

被引：15
|
作者：
Yu, Ya [1 ]
Qiao, Ang [1 ,2 ]
Bumstead, Alice Mary [3 ]
Bennett, Thomas D. [3 ]
Yue, Yuanzheng [1 ,2 ]
Tao, Haizheng [1 ]
机构：
[1] Wuhan Univ Technol, State Key Lab Silicate Mat Architectures, Wuhan 430070, Peoples R China
[2] Aalborg Univ, Dept Chem & Biosci, DK-9220 Aalborg, Denmark
[3] Univ Cambridge, Dept Mat Sci & Met, Cambridge CB3 0FS, England
来源：
CRYSTAL GROWTH & DESIGN | 2020年 / 20卷 / 10期
基金：
英国工程与自然科学研究理事会;
关键词：
METAL-ORGANIC FRAMEWORKS; STABILITY;
D O I：
10.1021/acs.cgd.0c00740
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
We show that 1-methylimidazole (1-MeIm) can act as a modulator for the synthesis of the zeolitic imidazolate framework ZIF-4 [Zn(Im)(2)], since it affects the particle size, size distribution, morphology, and surface defects of the resultant product. This modulation has a strong impact on the polyamorphic phase transition, recrystallization, melting, and glass formation in ZIF-4 according to our detailed structural analysis and differential scanning calorimetric analysis. This work provides an effective route to tailor ZIF crystals with the desired characteristics and functionalities.
引用
收藏
页码：6528 / 6534
页数：7
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