Effect of extrusion parameters on microstructure and mechanical properties of Mg-7.5Gd-2.5Y-3.5Zn-0.9Ca-0.4Zr (wt%) alloy

被引:72
作者
Xu, C. [1 ,2 ]
Nakata, T. [2 ]
Qiao, X. G. [1 ]
Jiang, H. S. [1 ]
Sun, W. T. [1 ]
Chi, Y. C. [1 ]
Zheng, M. Y. [1 ]
Kamado, S. [2 ]
机构
[1] Harbin Inst Technol, Sch Mat Sci & Engn, Harbin 150001, Peoples R China
[2] Nagaoka Univ Technol, Res Ctr Adv Magnesium Technol, Nagaoka, Niigata 9402188, Japan
来源
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING | 2017年 / 685卷
基金
中国国家自然科学基金;
关键词
Magnesium alloys; Dynamic recrystallization; LPSO phase; Precipitation; Mechanical properties; ZN-ZR ALLOY; RARE-EARTH-ELEMENTS; GRAIN-SIZE; DYNAMIC RECRYSTALLIZATION; TEXTURE DEVELOPMENT; HEAT-TREATMENT; MG ALLOYS; GD; MAGNESIUM; EVOLUTION;
D O I
10.1016/j.msea.2016.12.121
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
As-cast Mg-7.5Gd-2.5Y-3.5Zn-0.9Ca-0.4Zr (wt%) alloy was indirectly extruded using different parameters. The microstructure, texture and mechanical properties of the as-extruded alloys were investigated. Hot extrusion effectively refines the microstructure and fragments the coarse phases in the as-cast alloy. The alloys extruded at 400 degrees C exhibit bimodal microstructure comprising fine dynamically recrystallized (DRXed) grains with weak basal texture and coarse worked grains with strong basal fiber texture. DRX process is promoted by increasing extrusion ratio. Extrusion at high temperatures of 450 degrees C and 500 C leads to complete DRX and weak basal fiber texture. In addition, DRXed grain growth occurs and an unusual texture with basal planes perpendicular to extrusion direction appears. The alloy extruded at 400 degrees C and ratio of 10:1 shows the tensile yield strength of 345 MPa, ultimate tensile strength of 405 MPa and elongation to failure of 8.8%. The strength decreases but elongation increases with increasing extrusion ratio and temperature, while the strain hardening capacity is improved due to the higher concentration of solute atom dissolved in the matrix, fewer dislocations and larger DRXed grain size.
引用
收藏
页码:159 / 167
页数:9
相关论文
共 36 条
[1]   Microstructural stability and grain growth kinetics in an extruded fine-grained Mg-Gd-Y-Zr alloy [J].
Alizadeh, R. ;
Mahmudi, R. ;
Ngan, A. H. W. ;
Langdon, T. G. .
JOURNAL OF MATERIALS SCIENCE, 2015, 50 (14) :4940-4951
[2]   An Unusual Extrusion Texture in Mg-Gd-Y-Zr Alloys [J].
Alizadeh, Reza ;
Mahmudi, Reza ;
Ngan, Alfonso H. W. ;
Langdon, Terence G. .
ADVANCED ENGINEERING MATERIALS, 2016, 18 (06) :1044-1049
[3]   Effect of heat treatment on strain hardening of ZK60 Mg alloy [J].
Chen, Xianhua ;
Pan, Fusheng ;
Mao, Jianjun ;
Wang, Jingfeng ;
Zhang, Dingfei ;
Tang, Aitao ;
Peng, Jian .
MATERIALS & DESIGN, 2011, 32 (03) :1526-1530
[4]   THE DEPENDENCE OF GRAIN-SIZE ON STRESS DURING DYNAMIC RECRYSTALLIZATION [J].
DERBY, B .
ACTA METALLURGICA ET MATERIALIA, 1991, 39 (05) :955-962
[5]   GDMG5 - A COMPLEX STRUCTURE WITH A LARGE CUBIC CELL [J].
FORNASINI, ML ;
MANFRINETTI, P ;
GSCHNEIDNER, KA .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1986, 42 :138-141
[6]   Effects of rare-earth elements Gd and Y on the solid solution strengthening of Mg alloys [J].
Gao, L. ;
Chen, R. S. ;
Han, E. H. .
JOURNAL OF ALLOYS AND COMPOUNDS, 2009, 481 (1-2) :379-384
[7]   Phase equilibria and transformations in ternary Mg-Gd-Zn alloys [J].
Groebner, Joachim ;
Kozlov, Artem ;
Fang, Xi-Ya ;
Zhu, Suming ;
Nie, Jian-Feng ;
Gibson, Mark A. ;
Schmid-Fetzer, Rainer .
ACTA MATERIALIA, 2015, 90 :400-416
[8]   Microstructure, mechanical properties, creep and corrosion resistance of Mg-Gd-Y-Zr(-Ca) alloys [J].
He, Shangming ;
Zeng, Xiaoqin ;
Peng, Liming ;
Guo, Xinwu ;
Chang, Jianwei ;
Ding, Wenjiang .
2006 BIMW: 2006 BEIJING INTERNATIONAL MATERIALS WEEK, PTS 1-4: MAGNESIUM, 2007, 546-549 :101-+
[9]   Effect of heat treatment on the stability of damping capacity in hypocutectic Mg-Si alloy [J].
Hu, XS ;
Wu, K ;
Zheng, MY .
SCRIPTA MATERIALIA, 2006, 54 (09) :1639-1643
[10]   Ultrahigh strength as-extruded Mg-10.3Zn-6.4Y-0.4Zr-0.5Ca alloy containing W phase [J].
Jiang, H. S. ;
Qiao, X. G. ;
Xu, C. ;
Zheng, M. Y. ;
Wu, K. ;
Kamado, S. .
MATERIALS & DESIGN, 2016, 108 :391-399