Morphologic characterization of DyxY1-xAl3(BO3)4 single crystals grown from the flux and vapour phase

被引:0
作者
Vázquez, RM
Caballero, MA
González-Mañas, M
Kokanyan, EP
Ruiz, CM
Diéguez, E
机构
[1] Univ Autonoma Madrid, Dept Fis Mat, E-28049 Madrid, Spain
[2] Natl Acad Sci, Inst Phys Res, Yerevan 375014, Armenia
[3] Univ Cadiz, Dept Cristalog & Mineral, Cadiz, Spain
关键词
nucleation; X-ray diffraction; X-ray topography; borates;
D O I
暂无
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
DyxY1-xAl3(BO3)(4) single crystals with different Dy concentrations from x = 0.001 to 0.1 have been grown from fluxed melts based on K2Mo3O10-B2O3 mixtures, in the temperature range from 1070degreesC to 900degreesC. Platelets of Dy:YAB have been obtained by evaporation from the melt that clearly showed both growth sectors and striations. Bulk crystal has been grown from the melt by spontaneous crystallization with good optical quality. Differential thermal analysis and X-ray diffraction have been used to study the behaviour of the initial mixed oxides, the growth conditions and the grown crystals. X-ray topography has been used to analyse the growth defects, the structure of the growth sectors and striations in the platelets. (C) 2002 Elsevier Science B.V. All rights reserved.
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页码:668 / 671
页数:4
相关论文
共 12 条
  • [1] Solid-state reactions in Y2O3:3Al2O3:4B2O3 system studied by FTIR spectroscopy and X-ray diffraction
    Beregi, E
    Watterich, A
    Kovács, L
    Madarász, J
    [J]. VIBRATIONAL SPECTROSCOPY, 2000, 22 (1-2) : 169 - 173
  • [2] HOLSA J, 1998, SPECTROCHIM ACTA A, V54, P398
  • [3] Continuous-wave laser properties of the self-frequency-doubling YAl3(BO3)4:Nd crystal
    Jaque, D
    Capmany, J
    Sole, JG
    Luo, ZD
    Jiang, AD
    [J]. JOURNAL OF THE OPTICAL SOCIETY OF AMERICA B-OPTICAL PHYSICS, 1998, 15 (06) : 1656 - 1662
  • [4] JUNG ST, 1996, MAT RES B, V31, P8
  • [5] Flux growth and luminescence of Ho:YAl3(BO3)4 and PrAl3(BO3)4 crystals
    Koporulina, EV
    Leonyuk, NI
    Hansen, D
    Bray, KL
    [J]. JOURNAL OF CRYSTAL GROWTH, 1998, 191 (04) : 767 - 773
  • [6] Flux growth, composition, structural and thermal characteristics of (RxY1-x)Al3(BO3)4 (R = Nd, Gd; x = 1, 0.6, 0.65, 0.7 and 0.75) crystals
    Koporulina, EV
    Leonyuk, NI
    Barilo, SN
    Kurnevich, LA
    Bychkov, GL
    Mokhov, AV
    Bocelli, G
    Righi, L
    [J]. JOURNAL OF CRYSTAL GROWTH, 1999, 198 : 460 - 465
  • [7] Recent developments in the growth of RM(3)(BO3)(4) crystals for science and modern applications applications
    Leonyuk, NI
    [J]. PROGRESS IN CRYSTAL GROWTH AND CHARACTERIZATION OF MATERIALS, 1995, 31 (3-4): : 279 - 312
  • [8] Recent developments in the growth of RM(3)(BO3)(4) crystals for science and modern applications applications
    Leonyuk, NI
    [J]. PROGRESS IN CRYSTAL GROWTH AND CHARACTERIZATION OF MATERIALS, 1995, 31 (3-4): : 279 - 312
  • [9] Crystal growth of solid solutions based on the YAl3(BO3)4, NdAl3(BO3)4 and GdAl3(BO3)4 borates
    Leonyuk, NI
    Koporulina, EV
    Barilo, SN
    Kurnevich, LA
    Bychkov, GL
    [J]. JOURNAL OF CRYSTAL GROWTH, 1998, 191 (1-2) : 135 - 142
  • [10] LIN JT, 1990, LASER OPTRON, V34