A Novel Method for Preparing Silanols from Silylmethanols

被引:0
|
作者
Takeda, Daisuke [1 ]
Oyama, Ryo [1 ]
Yamada, Shozo [1 ]
机构
[1] Taiho Pharmaceut Co Ltd, CMC Ctr, Chem Technol Lab, Kamikawa, Saitama 3670241, Japan
关键词
HETEROGENEOUS OXIDATION; ORGANOSILANES; CONVERSION; ALKENYLSILANOLS; DERIVATIVES; ARYL;
D O I
10.1246/cl.2009.532
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Various types of silylmethanols were converted into their corresponding silanols in good to excellent yield under mild oxidation conditions using TEMPO (2,2,6,6-tetramethyl-1-piperidinyloxyl).
引用
收藏
页码:532 / 533
页数:2
相关论文
共 50 条
  • [31] A novel method to synthesize vanadium nitride nanopowders by ammonia reduction from combustion precursors
    Qin, Mingli
    Wu, Haoyang
    Cao, Zhiqin
    Zhang, Deyin
    Jia, Baorui
    Qu, Xuanhui
    JOURNAL OF ALLOYS AND COMPOUNDS, 2019, 772 : 808 - 813
  • [32] Novel skeletal rearrangements of a diterpene derived from deltaline
    Tang, Pei
    Wang, Ling
    Chen, Qi-Feng
    Chen, Qiao-Hong
    Jian, Xi-Xian
    Wang, Feng-Peng
    TETRAHEDRON, 2012, 68 (31) : 6249 - 6256
  • [33] Highly Efficient and Novel Method for Synthesis of 1,3,5-Triarylbenzenes from Acetophenones
    Phatangare, Kiran
    Padalkar, Vikas
    Mhatre, Devidas
    Patil, Ketan
    Chaskar, Atul
    SYNTHETIC COMMUNICATIONS, 2009, 39 (22) : 4117 - 4121
  • [34] A Novel and Rapid Method to Prepare Aminothiazoles
    Raut, Dattatraya
    Bhosale, Dnyandev
    Bhosale, Raghunath
    Lawand, Anjana
    Hublikar, Mahesh
    Edake, Nagesh
    Deshmukh, Sandip
    Hiwarale, Dipak
    ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 2025, 57 (02) : 172 - 176
  • [35] Novel processes for preparing high-purity anhydrous YCl3 and Mg-Y alloys
    Pan, Binfeng
    Liu, Jie
    Zhang, Zhimin
    Lu, Xuchen
    MATERIALS AND MANUFACTURING PROCESSES, 2025, 40 (07) : 943 - 950
  • [36] A novel catalyst-free method for the synthesis of mono-N-substituted thioureas in water
    Kaboudin, Babak
    Hajmohammadi, Elham
    Sohrabi, Masoumeh
    Kazemi, Foad
    JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2024, 21 (02) : 561 - 567
  • [37] A Novel Synthesis Method of Zeolite X From Coal Fly Ash: Alkaline Fusion Followed by Ultrasonic-Assisted Synthesis Method
    Ozdemir, Ozgul Dere
    Piskin, Sabriye
    WASTE AND BIOMASS VALORIZATION, 2019, 10 (01) : 143 - 154
  • [38] A novel method for the synthesis of 3,4-disubstitutedpyrrole-2,5-dicarboxylates from hydrazones derived from α-diazo esters
    Yasui, Eiko
    Wada, Masao
    Nagumo, Shinji
    Takamura, Norio
    TETRAHEDRON, 2013, 69 (21) : 4325 - 4330
  • [39] Optimization of Reaction Conditions for Preparing Carboxymethyl Cellulose from Corn Cobic Agricultural Waste
    Singh, Raj Kumar
    Singh, Arun Kumar
    WASTE AND BIOMASS VALORIZATION, 2013, 4 (01) : 129 - 137
  • [40] Synergistic effect of silanols in mesopores leading to unexpected catalysis of dendritic mesoporous silica particles in the aqueous-phase synthesis of 5-hydroxymethylfurfural from fructose
    Khoonsap, Santi
    Buengkitcharoen, Lalita
    Amnuaypanich, Sujitra
    Thongnoppakhun, Natthaya
    Patdhanagul, Nopbhasinthu
    Suthirakun, Suwit
    Sukpattanacharoen, Chattarika
    Amnuaypanich, Sittipong
    CHEMICAL ENGINEERING JOURNAL, 2023, 477