Synthesis of strapped nickel(II) macrocyclic complex of tetraaza[14]annulene

被引：0
|
作者：
Singh, R [1 ]
Bhattacharya, A [1 ]
Kumar, P [1 ]
机构：
[1] Gurukula Kangri Univ, Dept Chem, Hardwar 249404, India
来源：
JOURNAL OF THE INDIAN CHEMICAL SOCIETY | 2002年 / 79卷 / 06期
关键词：
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A description has been made of the reaction of 7,12-dimethyl-5,14 diphenyidibenzo[b,i][1,4,8,11[tetrauzacyclodetracinatonickel(ii) further denoted tetraaza[14]annulenenickel(u) with 3,3-(2,6-pyridinedioxy)dibenzoyl chloride hydrochloride which afforded the corresponding strapped Ni-II complex containing an interactive pyridine group. The infrared spectrum showed the presence of the C=O stretching band at 1670 cm(-1) and of the C-O-C stretching bands at 1054 and 1228 cm(-1). The structure of the strapped macrocyclic complex is confirmed by elemental and spectral analysis.
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页码：525 / 526
页数：2
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