Long chain polymer assisted synthesis of flower-like cadmium sulfide nanorods via hydrothermal process

被引:134
作者
Salavati-Niasari, Masoud [1 ,2 ]
Davar, Fatemeh [1 ,2 ]
Loghman-Estarki, Mohammad Reza [1 ]
机构
[1] Univ Kashan, Inst Nanosci & Nanotechnol, Kashan, Iran
[2] Univ Kashan, Dept Chem, Fac Sci, Kashan, Iran
关键词
Nanostructures; Semiconductors; Chemical synthesis; Optical spectroscopy; ZNO NANORODS; NANOWIRES; CDS; NANOPARTICLES; NANOCRYSTALS; ROUTE; MORPHOLOGIES; SURFACE;
D O I
10.1016/j.jallcom.2009.03.086
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Flower-like CdS nanostructure was obtained by a PEG2000 and thioglycolic acid (TGA) assisted hydrothermal process at relatively low temperature. Products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), ultraviolet-visible (UV-vis) spectroscopy, photoluminescence spectroscopy (PL), Fourier transform infrared (FT-IR) spectra, and thermogravimetric-differential thermal analysis (TG-DTA). Results show that TGA played a significant role in the formation of US nanostructures. A preliminary explanation of the mechanism is proposed. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:776 / 780
页数:5
相关论文
共 27 条
[1]   Calorimetric investigation of the formation of ZnS nanoparticles in W/O microemulsions [J].
Arcoleo, V ;
Goffredi, M ;
Liveri, VT .
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 1998, 51 (01) :125-133
[2]   Low-temperature synthesis and optical properties of wurtzite ZnS nanowires [J].
Cheng, Chuanwei ;
Xu, Guoyue ;
Zhang, Haiqian ;
Cao, Jieming ;
Jiao, Peipei ;
Wang, Xiaoxia .
MATERIALS LETTERS, 2006, 60 (29-30) :3561-3564
[3]   Theoretical characterization of triangular CdS nanocrystals:: A tight-binding approach [J].
Díaz, JG ;
Planelles, J .
LANGMUIR, 2004, 20 (25) :11278-11284
[4]   On some organic inhibitors of zinc corrosion in alkaline media [J].
Dobryszycki, J ;
Biallozor, S .
CORROSION SCIENCE, 2001, 43 (07) :1309-1319
[5]   Applied physics - Nanowires: Small is beautiful [J].
Fasol, G .
SCIENCE, 1998, 280 (5363) :545-546
[6]  
Fokerov V.A., 2004, PHYS REV LETT, V92
[7]  
Fonoberov VA, 2002, PHYS REV B, V66, DOI 10.1103/PhysRevB.66.085310
[8]   Strongly photoluminescent CdTe nanocrystals by proper surface modification [J].
Gao, MY ;
Kirstein, S ;
Möhwald, H ;
Rogach, AL ;
Kornowski, A ;
Eychmüller, A ;
Weller, H .
JOURNAL OF PHYSICAL CHEMISTRY B, 1998, 102 (43) :8360-8363
[9]  
GUOYUE X, 2006, T NONFERR METAL SOC, V16, P105
[10]   Fabrication of CuS nanocrystals with various morphologies in the presence of a nonionic surfactant [J].
Ji, HM ;
Cao, JM ;
Feng, J ;
Chang, X ;
Ma, XJ ;
Liu, JS ;
Zheng, MB .
MATERIALS LETTERS, 2005, 59 (24-25) :3169-3172