Synthesis and characterization of single crystalline PbO nanorods via a facile hydrothermal method

被引：38

作者：

Jia, Baoping ^{[1
]}

Gao, Lian ^{[1
]}

机构：

[1] Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China

来源：

MATERIALS CHEMISTRY AND PHYSICS | 2006年 / 100卷 / 2-3期

关键词：

inorganic compounds; nanostructure; chemical synthesis; microstructure; CARBON NANOTUBES; NANOCRYSTALS; NANOWIRES;

D O I：

10.1016/j.matchemphys.2006.01.012

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Single crystalline beta-PbO nanorods with diameter range from 40 to 120 nm and length up to 500 nm have been synthesized via a facile hydrothermal method in the presence of citrate. X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electro-microscope (HRTEM) and SAED were used to characterize the as-obtained samples. An interesting intermediate state of self-assembled beta-PbO rod-like nanoparticles was found and the possible formation mechanism of single crystalline beta-PbO nanorods was also discussed. (c) 2006 Elsevier B.V. All rights reserved.

引用

页码：351 / 354

页数：4

共 20 条

[1] CAPILLARITY-INDUCED FILLING OF CARBON NANOTUBES [J].