Optimized pinhole geometry for small-angle scattering

被引:20
作者
Wacha, Andras [1 ]
机构
[1] Hungarian Acad Sci, Res Ctr Nat Sci, Budapest, Hungary
来源
JOURNAL OF APPLIED CRYSTALLOGRAPHY | 2015年 / 48卷
关键词
small-angle X-ray scattering (SAXS); collimation; pinholes; small-angle scattering (SAS); parasitic scattering; signal-to-noise ratio; X-RAY-SCATTERING; CAMERA; BEAMLINE; COLLIMATION; INSTRUMENT; CONTRACTION; SENSITIVITY; RESOLUTION; APPARATUS; SYSTEM;
D O I
10.1107/S1600576715018932
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
In order to make the most of the low photon flux in laboratory small-angle X-ray scattering instruments, the experimental geometry has to be chosen carefully, with special stress on the beam-shaping system. The optimum collimation scheme should enable accurate measurements over the desired range of the scattering variable, while yielding the highest flux and the lowest possible instrumental background. In order to identify the best setting, a phase-space optimization of the collimating scheme is carried out in the present work, including constraints on the beam size at the sample position and on the detector surface. The resulting formulae are implemented in a Python script with a graphical user interface, to aid the planning, construction and daily operation of pinhole small-angle scattering cameras.
引用
收藏
页码:1843 / 1848
页数:6
相关论文
共 26 条
  • [1] Versatile sample environments and automation for biological solution X-ray scattering experiments at the P12 beamline (PETRA III, DESY)
    Blanchet, Clement E.
    Spilotros, Alessandro
    Schwemmer, Frank
    Graewert, Melissa A.
    Kikhney, Alexey
    Jeffries, Cy M.
    Franke, Daniel
    Mark, Daniel
    Zengerle, Roland
    Cipriani, Florent
    Fiedler, Stefan
    Roessle, Manfred
    Svergun, Dmitri I.
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2015, 48 : 431 - 443
  • [2] EFFECTIVE USE OF COLLIMATING APERTURES IN SMALL-ANGLE X-RAY DIFFRACTION CAMERAS
    BOLDUAN, OEA
    BEAR, RS
    [J]. JOURNAL OF APPLIED PHYSICS, 1949, 20 (10) : 983 - 992
  • [3] Development of powder diffraction apparatus for small-angle X-ray scattering measurements
    Bota, Attila
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2013, 46 : 573 - 576
  • [4] A small-angle X-ray scattering apparatus for studying biological macromolecules in solution
    Bu, ZM
    Perlo, A
    Johnson, GE
    Olack, G
    Engelman, DM
    Wyckoff, HW
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1998, 31 : 533 - 543
  • [5] SAXS instruments with slit collimation: investigation of resolution and flux
    Fritz, G
    Bergmann, A
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2006, 39 : 64 - 71
  • [6] JUSIFA - A NEW USER-DEDICATED ASAXS BEAMLINE FOR MATERIALS SCIENCE
    HAUBOLD, HG
    GRUENHAGEN, K
    WAGENER, M
    JUNGBLUTH, H
    HEER, H
    PFEIL, A
    RONGEN, H
    BRANDENBERG, G
    MOELLER, R
    MATZERATH, J
    HILLER, P
    HALLING, H
    [J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 1989, 60 (07) : 1943 - 1946
  • [7] ORNL 10-METER SMALL-ANGLE X-RAY-SCATTERING CAMERA
    HENDRICKS, RW
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1978, 11 (FEB) : 15 - 30
  • [8] Matplotlib: A 2D graphics environment
    Hunter, John D.
    [J]. COMPUTING IN SCIENCE & ENGINEERING, 2007, 9 (03) : 90 - 95
  • [9] CONSTANCY OF AXIAL SPACINGS IN FROG SARTORIUS MUSCLE DURING CONTRACTION
    HUXLEY, HE
    BROWN, W
    HOLMES, KC
    [J]. NATURE, 1965, 206 (4991) : 1358 - &
  • [10] LOW-ANGLE X-RAY DIAGRAM OF VERTEBRATE STRIATED MUSCLE AND ITS BEHAVIOUR DURING CONTRACTION AND RIGOR
    HUXLEY, HE
    BROWN, W
    [J]. JOURNAL OF MOLECULAR BIOLOGY, 1967, 30 (02) : 383 - &