Synthesis and characterization of SrFeO3-δ nanoparticles as antimicrobial agent

被引:61
作者
Abdel-Khalek, E. K. [1 ]
Rayan, D. A. [2 ]
Askar, Ahmed. A. [3 ]
Maksoud, M. I. A. Abdel [4 ]
El-Bahnasawy, H. H. [1 ]
机构
[1] Al Azhar Univ, Fac Sci, Dept Phys, Cairo 11884, Egypt
[2] Cent Met Res & Dev Inst CMRDI, POB 87, Cairo 11421, Egypt
[3] Al Azhar Univ, Fac Sci Boys, Bot & Microbiol Dept, Cairo, Egypt
[4] Atom Energy Author, Natl Ctr Radiat Res & Technol NCRRT, Radiat Phys Dept, Mat Sci Lab, Cairo, Egypt
关键词
SrFeO3-delta; Thermal; optical; Magnetic; Antimicrobial properties; MAGNETIC-PROPERTIES; PHOTOELECTRON-SPECTROSCOPY; X-RAY; PEROVSKITE; PERFORMANCE; CHEMISTRY;
D O I
10.1007/s10971-020-05431-8
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this work, synthesis and characterization of SrFeO3-delta nanoparticles as antimicrobial agent are presented. Structural characterization of SrFeO3-delta sample shows that it has a cubic (Pm3m) phase with minor tetragonal phase. The morphology of the SrFeO3-delta nanoparticles sample was characterized by a field emission scanning electron microscope (FE-SEM) and high resolution transmission electron microscopy (HRTEM). Mossbauer spectroscopy and X-ray photoelectron spectroscopy (XPS) results showed that the iron exists in oxidation states Fe3+, Fe3.5+, and Fe4+. The SrFeO3-delta nanoparticles sample exhibits energy band gap (E-g = 1.75 eV) which lies in the Visible region. Thermal and magnetic studies provide an evidence for ferroelectricity and antiferromagnetic with small amount of ferromagnetic in SrFeO3-delta nanoparticles sample, respectively. SrFeO3-delta nanoparticles sample showing powerful activity to fight both of tested Gram-positive, Gram-negative bacteria, and fungi strains. The antimicrobial activity as well as the minimal inhibitory concentration (MIC) and the minimum bactericidal concentration (MBC) of the SrFeO3-delta nanoparticles sample have been investigated.
引用
收藏
页码:27 / 38
页数:12
相关论文
共 53 条
[1]   Structural, optical, dielectric and magnetic properties of Bi1-xLaxFeO3 nanoparticles [J].
Abdel-Khalek, E. K. ;
Ibrahim, Islam ;
Salama, Tarek M. ;
Elseman, Ahmed M. ;
Mohamed, Mohamed Mokhtar .
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2018, 465 :309-315
[2]   Magnetoresistance effects in SrFeO3-δ:: Dependence on phase composition and relation to magnetic and charge order [J].
Adler, P ;
Lebon, A ;
Damljanovic, V ;
Ulrich, C ;
Bernhard, C ;
Boris, AV ;
Maljuk, A ;
Lin, CT ;
Keimer, B .
PHYSICAL REVIEW B, 2006, 73 (09)
[3]   Structural studies of SrFeO3 and SrFe0.5Nb0.5O3 by employing XRD and XANES spectroscopic techniques [J].
Akhtar, M. Javed ;
Khan, R. Tahir Ali .
MATERIALS CHARACTERIZATION, 2011, 62 (10) :1016-1020
[4]   Pyridine azo disperse dye derivatives and their selenium nanoparticles (SeNPs): synthesis, fastness properties, and antimicrobial evaluations [J].
Alnassar, Huda S. A. ;
Helal, Maher H. E. ;
Askar, Ahmed A. ;
Masoud, Doaa M. ;
Abdallah, Amira E. M. .
INTERNATIONAL JOURNAL OF NANOMEDICINE, 2019, 14 :7903-7918
[5]   Design, synthesis, antimicrobial activity and molecular docking studies of some novel di-substituted sulfonylquinoxaline derivatives [J].
Ammar, Yousry A. ;
Farag, Awatef A. ;
Ali, Abeer M. ;
Ragab, Ahmed ;
Askar, Ahmed A. ;
Elsisi, Doaa M. ;
Belal, Amany .
BIOORGANIC CHEMISTRY, 2020, 104
[6]  
ATEIA EE, 2017, APPL PHYS A MATER, V123
[7]   Structural, electrical and electrochemical properties of co-precipitated SrFeO3-δ [J].
Augustin, CO ;
Berchmans, LJ ;
Selvan, RK .
MATERIALS LETTERS, 2004, 58 (7-8) :1260-1266
[8]   Mechanosynthesis and magnetic properties of nanocrystalline LaFeO3 using different iron oxides [J].
Cristobal, A. A. ;
Botta, P. M. ;
Bercoff, P. G. ;
Porto Lopez, J. M. .
MATERIALS RESEARCH BULLETIN, 2009, 44 (05) :1036-1040
[9]   Synthesis and antimicrobial evaluation of amino sugar-based naphthoquinones and isoquinoline-5,8-diones and their halogenated compounds [J].
Dias, Flaviana R. F. ;
Novais, Juliana S. ;
do Nascimento Santos Devillart, Talita A. ;
da Silva, Wanderson Amaral ;
Ferreira, Matheus O. ;
Loureiro, Raquel de S. ;
Campos, Vinicius R. ;
Ferreira, Vitor F. ;
de Souza, Maria C. B. V. ;
Castro, Helena C. ;
Cunha, Anna C. .
EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2018, 156 :1-12
[10]   Highly crystalline strontium ferrites SrFeO3-δ: an easy and effective wet-chemistry synthesis [J].
Diodati, S. ;
Nodari, L. ;
Natile, M. M. ;
Russo, U. ;
Tondello, E. ;
Lutterotti, L. ;
Gross, S. .
DALTON TRANSACTIONS, 2012, 41 (18) :5517-5525