Shrinkage control of yttria-stabilized zirconia during ac electric field-assisted sintering

Yttria-stabilized zirconia pellets were easily and accurately sintered to a predetermined sintering level, including near full density, in an experimental arrangement consisting of a vertical dilatometer and an ac adjustable power supply. Conventional and electric field-assisted sintering steps can be combined, starting from temperatures above 800 degrees C and applying 1000 Hz alternating electric fields in the range 80-160 V cm(-1). A systematic comparison of the microstructures and impedance diagrams of samples conventionally and electric field-assisted sintered to the same density levels shows that the non-conventional sintering method gives significantly small grains in agreement with previous observations. The results show that this sintering method can be applied to produce materials partially sintered at any desired shrinkage level. (C)0 2014 Elsevier Ltd. All rights reserved.