Dielectric properties evaluation of NiFe2O4/MWCNTs nanohybrid for microwave applications prepared via novel one step synthesis

被引:27
作者
Soomro, Sumair Ahmed [1 ]
Gut, Iftikhar Hussain [1 ]
Khan, Muhammad Zarrar [1 ]
Naseer, Hashim [1 ]
Khan, Ahmad Nawaz [1 ]
机构
[1] NUST, SCME, TTL, Dept Mat Engn ME, H-12 Campus, Islamabad, Pakistan
关键词
AC conductivity; AC impedance spectroscopy; Dielectric properties; Fourier transform infrared spectroscopy; Nanomaterials; Scanning electron microscopy; ELECTRICAL-CONDUCTIVITY; ABSORBING PROPERTIES; FERRITE; COMPOSITES; ABSORPTION;
D O I
10.1016/j.ceramint.2016.12.002
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
NiFe2O4/MWCNTs nanohybrids were synthesized via novel one step ultrasonication assisted method using ortho-xylene as a dispersive medium with varying MWCNTs concentration (0.0%, 1.0%, 1.5%, 2.0% and 2.5%). The nanohybrids were characterized by X-Ray Diffraction (XRD), Scanning Electron Microscope (SEM), Fourier Transform Infrared Spectroscopy (FT-IR) and Impedance Analyzer techniques. XRD indexed patterns confirmed the formation of NiFe2O4/MWCNTs nanohybrid. The SEM images showed the decoration of nickel ferrite nanoparticles on MWCNTs. The FTIR results show two absorption bands. The Cole-Cole plots of impedance show the resistance was only due to the grain boundary contribution. The dielectric properties were found to be increasing with increasing MWCNTs concentration. For 2.5% MWCNTs concentration, dielectric constant and loss 1.06x10(5), 1.99x10(6) were achieved as compared to pure nickel ferrite 6.17x10(3), 3.87x10(4), respectively. Such increase in the dielectric properties renders its application at high frequency
引用
收藏
页码:4090 / 4095
页数:6
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