Synthesis and characterization of acetylferrocenyl thiosemicarbazone derivatives of dichlorobis(cyclopentadienyl)hafnium(IV)

被引：0
|
作者：
Sengupta, SK [1 ]
Pandey, OP [1 ]
Bhatt, A [1 ]
Srivastava, V [1 ]
Mishra, KN [1 ]
机构：
[1] DDU Gorakhpur Univ, Dept Chem, Gorakhpur 273009, Uttar Pradesh, India
来源：
INDIAN JOURNAL OF CHEMISTRY SECTION A-INORGANIC BIO-INORGANIC PHYSICAL THEORETICAL & ANALYTICAL CHEMISTRY | 2002年 / 41卷 / 07期
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中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The reactions of Cp2HfCl2 with thiosemicarbazones (LH) derived from acetylferrocene and substituted thiosemicarbazide (phenyl/4-chlorophenyl/4-nitrophenyl/4-inethylphenyl thiosemicarbazide) in various stoichiometric ratios have been studied and the complexes of the type [Cp2HfCl(L)] are obtained. Tentative structural conclusions are drawn for the reaction products based upon elemental analyses, electrical conductance, magnetic moment and spectral data (UV-Vis, IR, H-1 NMR and C-13 NMR).
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页码：1421 / 1423
页数：3
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