Synthesis of nanocomposite with a coreshell structure based on Fe3O4 magnetic nanoparticles and iron glycerolate

被引：8

作者：

Demin, A. M. ^{[1
]}

Khonina, T. G. ^{[1
]}

Shadrina, E., V ^{[1
]}

Bogdanova, E. A. ^{[2
]}

Kuznetsov, D. K. ^{[3
]}

Mekhaev, A., V ^{[1
]}

Shur, V. Ya ^{[3
]}

Krasnov, V. P. ^{[1
]}

机构：

[1] Russian Acad Sci, Ural Branch, Postovsky Inst Organ Synth, 22 Ul S Kovalevskoi, Ekaterinburg 620990, Russia

[2] Russian Acad Sci, Ural Branch, Inst Solid State Chem, 91 Ul Pervomaiskaya, Ekaterinburg 620990, Russia

[3] Ural Fed Univ, Inst Nat Sci & Math, 51 Prosp Lenina, Ekaterinburg 620000, Russia

来源：

RUSSIAN CHEMICAL BULLETIN | 2019年 / 68卷 / 06期

关键词：

magnetic nanoparticles; iron glycerolate; nanocomposites; OXIDE NANOPARTICLES; IMMOBILIZATION; PMIDA; ZINC;

D O I：

10.1007/s11172-019-2536-x

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An original method for preparation of nanoparticles with a coreshell structure based on Fe3O4 magnetic nanoparticles (MNPs) and iron glycerolate was proposed. The formation of a coating on the MNP surface with a diameter of 11 nm was carried out by heating them in glycerol at 220 degrees C for 40 h. The synthesized nanoparticles were characterized using scanning transmission electron microscopy, XRD and IR spectroscopy. The amount of glycerol fragments in the nanocomposite calculated from the elemental analysis and TGA was 3.6 mmol per 1 g of MNPs (32.08 wt.%).

引用

页码：1178 / 1182

页数：5

共 20 条

[1]

[Anonymous], 2017, Pat. RF, Patent No. 2623153

[2] Targeted superparamagnetic iron oxide nanoparticles for early detection of cancer: Possibilities and challenges [J].

Bakhtiary, Zahra ;

Saei, Amir Ata ;

Hajipour, Mohammad J. ;

Raoufi, Mohammad ;

Vermesh, Ophir ;

Mahmoudi, Morteza .

NANOMEDICINE-NANOTECHNOLOGY BIOLOGY AND MEDICINE, 2016, 12 (02) :287-307

[3] IR AND MOSSBAUER STUDY OF IRON GLYCEROLATES [J].

BRUYLANTS, P ;

MUNAUT, A ;

PONCELET, G ;

LADRIERE, J ;

MEYERS, J ;

FRIPIAT, J .

JOURNAL OF INORGANIC & NUCLEAR CHEMISTRY, 1980, 42 (11) :1603-1611

[4] Silicon-boron-containing glycerohydrogel having wound healing, regenerative, and antimicrobial activity [J].

Chupakhin, O. N. ;

Khonina, T. G. ;

Kungurov, N. V. ;

Zilberberg, N. V. ;

Evstigneeva, N. P. ;

Kokhan, M. M. ;

Polishchuk, A. I. ;

Shadrina, E. V. ;

Larchenko, E. Yu. ;

Larionov, L. P. ;

Karabanalov, M. S. .

RUSSIAN CHEMICAL BULLETIN, 2017, 66 (03) :558-563

[5] Immobilization of fluorescent protein TagGFP2 on Fe3O4-based magnetic nanoparticles [J].

Demin, A. M. ;

Valova, M. S. ;

Pershina, A. G. ;

Krasnov, V. P. .

RUSSIAN CHEMICAL BULLETIN, 2019, 68 (05) :1088-1095

[6] pHLIP-modified magnetic nanoparticles for targeting acidic diseased tissue [J].

Demin, A. M. ;

Pershina, A. G. ;

Nevskaya, K. V. ;

Efimova, L. V. ;

Shchegoleva, N. N. ;

Uimin, M. A. ;

Kuznetsov, D. K. ;

Shur, V. Ya. ;

Krasnov, V. P. ;

Ogorodova, L. M. .

RSC ADVANCES, 2016, 6 (65) :60196-60199

[7] Immobilization of PMIDA on Fe3O4 magnetic nanoparticles surface: Mechanism of bonding [J].

Demin, Alexander M. ;

Mekhaev, Alexander V. ;

Esin, Alexander A. ;

Kuznetsov, Dmitry K. ;

Zelenovskiy, Pavel S. ;

Shur, Vladimir Ya. ;

Krasnov, Victor P. .

APPLIED SURFACE SCIENCE, 2018, 440 :1196-1203

[8] PMIDA-Modified Fe3O4 Magnetic Nanoparticles: Synthesis and Application for Liver MRI [J].

Demin, Alexander M. ;

Pershina, Alexandra G. ;

Minin, Artem S. ;

Mekhaev, Alexander, V ;

Ivanov, Vladimir V. ;

Lezhava, Sofiya P. ;

Zakharova, Alexandra A. ;

Byzov, Iliya, V ;

Uimin, Mikhail A. ;

Krasnov, Victor P. ;

Ogorodova, Ludmila M. .

LANGMUIR, 2018, 34 (11) :3449-3458

[9] 3-Aminopropylsilane-modified iron oxide nanoparticles for contrast-enhanced magnetic resonance imaging of liver lesions induced by Opisthorchis felineus [J].

Demin, Alexander M. ;

Pershina, Alexandra G. ;

Ivanov, Vladimir V. ;

Nevskaya, Kseniya V. ;

Shevelev, Oleg B. ;

Minin, Artyom S. ;

Byzov, Iliya V. ;

Sazonov, Alexey E. ;

Krasnov, Victor P. ;

Ogorodova, Ludmila M. .

INTERNATIONAL JOURNAL OF NANOMEDICINE, 2016, 11 :4451-4463

[10] Functionalization of Fe3O4 magnetic nanoparticles with RGD peptide derivatives [J].

Demin, Alexander M. ;

Vigorov, Alexey Yu. ;

Nizova, Irina A. ;

Uimin, Mikhail A. ;

Shchegoleva, Nina N. ;

Ermakov, Anatoly E. ;

Krasnov, Victor P. ;

Charushin, Valery N. .

MENDELEEV COMMUNICATIONS, 2014, 24 (01) :20-22

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